RussianPatents.com
|
Method for forming chitosan film coating and chitosan film coating. RU patent 2461575. |
|
FIELD: medicine. SUBSTANCE: chitosan is dissolved in an organic acid: 4-6% citric acid or 2-8% lactic acid in the relation of the ingredients chitosan: the organic acid 1:2-1:4 to prepare a forming solution. Chitosan has molecular weight 80-500 kDa. The forming solution is added with vitamin B1 in the amount of max. 0.5 wt %. The prepared forming solution is applied on a substrate in the amount of 0.2-0.25 ml/cm2 and kept to achieve a film structure. Said method is used to form the chitosan film coating having the thickness of 50-250 mcm and the breaking elongation of 42 to 470%. EFFECT: group of inventions allows preparing high-elastic chitosan citrate or lactate films possessing bactericidal action. 2 cl, 1 tbl, 13 ex
|
Wrapper tape / 2459841 Wrapper tape is made from a high-pressure polyethylene-based composition via extrusion, calendering, exposure to a stream of accelerated electrons and alignment in the longitudinal direction by 3-10% at temperature 60-85°C. Besides high-pressure polyethylene, the composition also contains a heat stabiliser of benzene propionic acid 3,5-bis (1,1 dimethylethyl) - 4-hydroxy-2-(3- (3,5-bis (1,1-dimethylethyl) - 4-hydroxyphenyl)-1-oxopropylhydrazide, light stabilisers, such as P-type soot - 2.0-2.5% and an oligomeric sterically hindered amine polymer of butanedionic acid with 4-hydroxy-2,2,6,6-tetramethyl-1-piperidine ethanol, and an elasticising additive based on regular butadiene-styrene thermoplastic rubber of the SBS type. |
Method of producing collodion film using centrifugal technique / 2458944 Invention relates to a method of producing films based on polymer materials and can be used in chemistry, biochemistry and medicine as a base for test systems in enzyme-immunoassay, as a base for chemical and biochemical sensors. The method of producing a collodion film using a centrifugal technique involves spraying a mixture of cellulose ester and an organic solvent onto a rotating surface. The mixture used is a solution of collodion in ethyl alcohol and diethyl ether, with the following ratio of components in vol. %: collodion 1; organic solvent - ethyl alcohol, diethyl ether 2-200, and the mixture is sprayed onto a rotating cylindrical surface. |
Pectin- and chitosan-based biodegradable film / 2458077 Biodegradable film contains pectin, chitosan, water, 1N hydrochloric acid, a plasticiser - glycerine and a structure-forming agent - 3% methyl cellulose solution. |
Collagenic materials, films and production methods thereof / 2455322 Invention relates to a collagenic film and a method of making said film. The film contains at least one collagenic layer. The surface of the collagenic layer is formed by a plurality of domains with predominant orientation of collagenic fibres in each domain and continuous variation of orientation of fibres from one domain to another. There are pores on the domain boundary. |
Polyolefin compositions / 2451699 Invention relates to polyolefin compositions for making films. The composition contains 55-80 wt % propylene homopolymer and 20-45 wt % copolymer of ethylene and one or more C4-C10-olefins, containing 10-40% of said C4-C10-olefin(s). The composition has melt flow rate MFR (230°C, 2.16 kg) from 1 to 4 g/10 min, overall content of ethylene from 20 wt % to 40 wt %, overall content of C4-C10 α-olefin(s) from 6 wt % to 15 wt % and ratio of overall content of ethylene to overall content of C4-C10 α-olefin(s) equal to or greater than 2.3. The overall content of a fraction which is soluble in xylene at room temperature ranges from 18 wt % to 30 wt %, and the modulus of elasticity in flexure, relating to the reactor-grade composition, is higher than 700 MPa. |
Polyolefin compositions having improved optical and mechanical properties / 2448992 Invention relates to polyolefin compositions and methods of producing said compositions. The polyolefin composition contains (A) a first propylene-ethylene random copolymer, having ethylene content CMA 1.0-6 wt % and melt flow rate MFR(A) 5-40 g/10 min and (B) a second propylene-ethylene random copolymer. The polyolefin composition has ethylene content CMAB 2.5-6 wt %, melt flow rate MFR(AB) 3-20 g/10 min, under the condition that CMAB>CMA and MFR(A)/MFR(AB)>1.45, and further has randomness R of ethylene distribution in the polymer chain ≥0.945. |
Polyethylene compositions, methods of producing said compositions and articles made therefrom / 2448991 Invention relates to films made from a polyethylene composition and articles made from said films, such as shipping bags and sheet material. The film contains at least one component made from the composition, which contains a mixture of an ethylene-based high-molecular weight copolymer and an ethylene-based low-molecular weight copolymer. The ethylene-based high-molecular weight copolymer is a heterogeneously branched linear or homogeneously branched linear ethylene copolymer and C3-C20 α-olefins having density from 0.922 g/cm3 to 0.929 g/cm3 and flow melt index at high load I21 from 0.2 g/10 min to 1.0 g/10 min. The ethylene-based low-molecular weight copolymer is a heterogeneously branched linear or homogeneously branched linear ethylene copolymer and C3-C20 α-olefins having density from 0.940 g/cm3 to 0.955 g/cm3 and flow melt index I2 from 6 g/10 min to 50 g/10 min. The mixture has a single peak on an ATREF curve, is eluted at temperature higher than 30°C, has viscosity-average molecular weight coefficient (CMV), which is calculated at elution temperature in the range from 70°C to 90°C, less than -0.0032 in coordinates of log(calculated MV) of elution temperature. |
Polyethylene compositions, having improved properties / 2448132 Polyethylene composition contains ethylene and butene and has long-chain branching index (g'av.) from 0.5 to 0.9; melt flow index (MFI) higher than (49.011×IR(-0.4304)), where IR is melt index; and ratio of weight-average molecular weight to number-average molecular weight Mw/Mn less than or equal to 4.6. The method for gas-phase polymerisation of olefins to obtain said composition is realised in the presence of a catalyst system containing an achiral cyclic bridge metallocene catalytic compound and an activator - aluminoxane, modified aluminoxane or mixture thereof. Films containing said composition have good optical and shrinking properties. In particular, a film can have one or more of the following characteristics: longitudinal plastic shrinkage stress (MD) ≤0.08 MPa; Retromat surface shrinkage >60%; transparency >60%; relative internal turbidity ≤1.0%/mil (i.e. %/0.001 inch); turbidity <20%. |
Composition of at least one vinylidene chloride polymer / 2447101 Invention relates to a vinylidene chloride polymer composition for making packaging film. The vinylidene polymer composition for making packaging film contains at least one vinylidene chloride polymer which is a vinylidene chloride homopolymer or copolymer; at least one e-caprolactone polymer from which at least one is characterised by that its molecular weight is less than or equal to 10000 g/mol; epoxidated soya bean oil; where the vinylidene chloride copolymer contains vinylidene chloride as the basic monomer and at least one comonomer selected from a group comprising vinyl chloride, vinyl esters, vinyl ethers, esters and amides of acrylic acids, esters and amides of methacrylic acids, acrylonitrile, methacrylonitrile, styrene, styrene derivatives, butadiene, olefins, such as, for example, ethylene and propylene, itaconic acid, maleic anhydride, 2-acrylamido-2-methylpropane sulphonic acid or one of salts thereof, phosphate ester of polypropylene glycol with terminal methacrylate groups. The invention also relates to a method of preparing the composition, which involves mixing the starting components; a method of making articles from films, foil, sheets, single- or multiple-layer films, or objects obtained by moulding, which involves extrusion of said composition. |
Polyethylene film having improved mechanical properties and impermeability, and method of making said film / 2447096 Invention relates to a polyethylene film for making packaging, grocery sacks, trash can liners and produce bags. The film is made from a multimodal polymer composition obtained using a double metallocene catalyst and contains an ethylene homopolymer or a copolymer of ethylene and alpha-olefin comonomer or combination thereof and, optionally, additives and modifiers. The film is characterised by total energy dart drop, measured in accordance with ASTM D4272, greater than about 0.45 ft.lbf, dart drop impact strength, measured in accordance with ASTM D1709 Method A, greater than about 135 g, and moisture vapour transmission rate, measured in accordance with ASTM F1249 at 100°F and 90% relative humidity, less than about 0.85 g-mil/100 square inch/24 hour. Said tests are performed on a test specimen having a 0.8 mil thickness. |
Method of producing chondroitin sulphate from sea hydrobiont tissue / 2458134 Method involves preparation of material for enzymatic hydrolysis. Alkaline hydrolysis is carried out with proteolytic enzyme preparations with neutralisation of the obtained solution to pH=7. A salt is added to the obtained enzymatic hydrolysate to a value of not less than 0.1 mol/l. Successive ultrafiltration is carried out, first on a membrane with maximum retention of 50 kD with separation of high-molecular weight impurities, and then on a membrane with maximum retention of 5 kD with separation of low-molecular weight substances. The chondroitin sulphate solution retained at the membrane is washed on the same membrane with distilled water until complete removal of salts. Final washing with distilled water is carried out on a membrane with maxim retention of 50 kD. |
Cross-linked hyaluronic acid and production method thereof / 2456299 Method involves activation of hyaluronic acid using a cross-linking agent and an auxiliary cross-linking agent. The activated hyaluronic acid then reacts with a nucleophilic cross-linking agent. The pH of the reaction medium ranges from 8 to 12. The nucleophilic cross-linking agent contains at least 50 wt % oligopeptide or polypeptide. Further, pH of the reaction medium is regulated to 5-7 and cross-linked hyaluronic acid is precipitated in the organic solvent. The invention also relates to use of the cross-linked hyaluronic acid obtained using this method in plastic surgery to make implants and to a hedrogel containing said cross-linked hyaluronic acid in a buffer aqueous solvent. |
Method of determining antibacterial activity of chitosan / 2450022 Disclosed is a method of determining antibacterial properties of chitosan by estimating its minimum bacteriostatic and/or bactericidal concentration. Complex buffer solutions based on three organic acids MES, ACES and TES with different pH values are prepared. The ready buffer solutions are poured into a vessel. Double dilutions of chitosan are then prepared in vessels with the buffer solutions. Aliquots of a bacterial suspension in a fluid medium are added to the chitosan solutions in the buffer. The solutions are incubated for 24 hours at temperature which is optimum for bacterial growth. The minimum bacteriostatic and/or minimum bactericidal concentration of chitosan is then determined after incubation by determining growth of the culture or a drop in the number of living cells, respectively. |
Method for preparing boron-containing hyaluronic acid / 2445978 Invention refers to a method for preparing sodium salt of hyaluronic acid modified by boron compounds with no fluid medium added. The method consists in the fact that powdered sodium salt of hyaluronic acid together with a modifying agent and mixed modifying agents is pre-homogenised in a mixer at temperature ranging within 20° to 50°C; thereafter the prepared homogenous powder mixture is simultaneously exposed to pressure and shearing deformation in a mechanochemical reactor at temperature ranging within 20° to 50°C and pressure 5-1000 MPa. |
Method for producing chitosan oligomers / 2445101 Invention refers to medicine, more specifically to producing chitosan oligomers possessing biological activity and applicable in food industry and medicine. In a method for producing chitosan oligomers, a chitosan solution is taken in the concentration of 0.025-0.075% (weight/volume) and exposed to low-frequency ultrasound of the intensity of 92-460 Wt/cm2 for 5-30 minutes. |
Method of producing d(+) glucosamine hydrochloride / 2440362 Method involves preliminary acetylation of chitin with acetic anhydride, washing and drying the acetylated chitin in order to reduce degree of deacetylation thereof and, as a result, increase output of the desired product - D(+)-glucosamine hydrochloride when obtaining said product through hydrolysis of acetylated chitin with concentrated hydrochloric acid while heating, followed by evaporation, crystallisation, separation, washing and drying the desired product. |
Chitosan chromate, synthesis method thereof and energy-intensive composition containing said chitosan chromate / 2439081 Method of producing chitosan chromate involves reaction of soluble chitosan salts with metal chromates in ratio of 2 moles of the chitosan cation to 1 mole of chromate anion or with metal bichromates in ratio of 4 moles of the chitosan cation to 1 mole of the bichromate anion. The solid chitosan chromate residue formed is then separated and dried at temperature not higher than 150°C. The invention discloses an energy-intensive composition based on chitosan dodecahydro-closo-dodecaborate containing an effective amount of chitosan chromate. The quantitative ratio in the energy-intensive composition is by the required combustion mode: the higher the content of chitosan chromate, the higher the activity of the composition. |
Method of determining degree of deacetylation of chitosan / 2436798 Method involves taking a certain weighed amount of chitosanium chromate which is first purified from extraneous impurities and reduced to constant weight. The weighed amount is then turned into a stable weighted form through thermal treatment on air at temperature 800-900°C to form chromium oxide Cr2O3. The weight of the formed chromium oxide is then determined. Content of chromic acid in the initial weighed amount of chitosanium chromate is then calculated from the weight of chromium oxide. The degree of deacetylation of chitosan is calculated using defined formulae. |
Method of extracting and stabilising low-molecular aminoglycans from eggshell wastes / 2435786 Invention relates to a method of extracting and stabilising ultra low-molecular aminoglycans from eggshell wastes. Aminoglycan extract is used to produce cosmetic creams with skin moisturising and anti-wrinkle properties. The method of extracting low-molecular aminoglycan compound of formula I from a natural source of eggshell wastes, which consists of alternating glucuronic acid and N-acetylglucosamine units, where M can be one or more of Na, Ca, K, Mg; and n is a whole number from 20 to 40, involves the following steps: (a) preparing eggshell wastes for extraction of embryonic low-molecular aminoglycan compound of formula I using a polar organic solvent in water, (b) extracting low-molecular aminoglycan compound of formula I in form of a water-soluble salt, for which the eggshell from step (a) is vigorously shaken with aqueous polar salt solution at 10°C - 35°C for 6-12 hours, then filtered or centrifuged in order to collect an aqueous layer containing a dissolved aminoglycan compound of formula I; (c) extracting a purified low-molecular aminoglycan compound of formula I by forming a gel from an aqueous mixture of salts using a polar organic solvent, for which the solution from step (b) is successively and step-by-step mixed with an organic solvent mixed with water while gently stirring and then cooled to maintain temperature from 20°C to 25°C, and the formed gel is left for 2-24 hours for complete precipitation, then filtered or centrifuged in order to extract a semidry aminoglycan compound of formula I; (d) the extracted aminoglycan compound of formula I from step (c) is stabilised via gradual addition of organic oils to the semidry gel to form aminoglycan compound of formula I. In order to prepare a composition having anti-wrinkle properties, at least one pharmaceutically acceptable filler is added to the stabilised aminoglycan compound of formula I obtained at step (d). |
Method and apparatus for treating fermented wastes and producing chitin containing biomass / 2430929 Method involves feeding wastes to be treated into artificial containers, biotreatement, tapping the filtrate and removing the obtained biomass. Biotreatement is carried out by culturing hoverfly larvae from the freshly laid eggs phase to the pupation phase in the fermented wastes to be treated, placed in artificial meshed containers the bottom and walls of which are covered with filter cloth. The apparatus has artificial containers, devices for feeding the wastes to be treated, outputting the filtrate and collecting the biomass. The artificial containers have a meshed bottom and walls covered with filter cloth. |
Method for producing of chitosan from chitin of cancerous / 2246880 Method involves providing deacetylation of raw material with the use of preliminarily cooled alkaline solution; washing and drying. Deacetylation process is performed in three stages, first stage being performed for 7 days and subsequent two stages being performed for 2 hours each, combined with thermal processing at temperature of 55-590C. Washing process is provided after each deacetylation stage. |
© 2013-2014 Russian business network RussianPatents.com - Special Russian commercial information project for world wide. Foreign filing in English. |