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Method for determination of pectin substances weight percentage in vegetal raw material. RU patent 2434532. |
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FIELD: food industry. SUBSTANCE: invention relates to food industry, in particular to determination of pectin substances quantity in vegetal raw material. The method envisages drying plaited paper filter until constant weight, preparation of protopectin and hydratopectin, sampling. The protopectin solution acid medium is neutralised with pectin substances fraction in the solutions being analysed saponified with 40% solution of NaOH during 15 minutes. Then pectin substances are sedimented with concentrated HCl and the sediment is filtered. Then the sediments on filters are washed with cold distilled water. Filters with sediments are dried till constant weight and one calculates pectin substances fractions weight percentage from certain formulas. EFFECT: invention enables enhanced accuracy of determination of pectin substances weight percentage in vegetal raw material, reduction of time and labour expenditures as well as specific equipment usage exclusion. 2 tbl, 2 ex
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Method for drying polysaccharides based on uronic acid / 2422045 Invention relates to food industry. In accordance with the method proposed one mixes a powder containing an uronic acid based oligosaccharide, water, protein and a carbohydrate to produce water solution heated to a temperature of 50 - 90°C. Then one adds fat to the heated solution and dries it by way of spraying to produce a powder composition. The uronic acid based oligosaccharide has DP 2 - 250. Additionally proposed is the powder produced by this method and a food product containing such powder. |
Method for production of pectin and food fibres of pumpkin cake / 2422044 Invention refers to food industry, and namely to pectin production. The method involves pumpkin cake washing with water, pressing and hydrolysis extraction, the mixture water duty being 1:(4-5), at a 60-65°C temperature during 60 minutes. The extragent used is anolyte with pH20 = 4.0-4.5. The hydrolysis mass is separated into cake and hydrolysate by way of pressing. The cake is extracted with catholite with pH20 = 7.5-8.0, the mixture water duty being 1:3, at a 60°C temperature during 30 minutes. Then the cake having been extracted is separated from the extract by way of pressing. Cake particles are milled and dried to produce food fibres. The extract is mixed with the hydrolysate and filtered. The mixture is delivered for alcohol precipitation of pectin and its during. The anolyte and the catholyte are produced by way of sodium chloride treatment in an diaphragm electrolyser. |
Meat substitute product production method; meat substitute product produced by this method and ready-to-use meat substitute product / 2417623 Invention is intended for use in food industry to produce a meat substitute product. The method involves the following stages: (1) a protein material, a hydrocolloid sedimented with metal cations and water are added to each other; (2) the compositions produced at stage (1) a homogeneous mixture is prepared; (3) the mixture produced at stage (2), while stirred, is blended with a metal cations solution which contains soluble calcium or magnesium salts or their mixture to form a fibrous product; (4) one separates the fibrous product; (5) the protein material contains a milk protein material chosen from the group consisting of dry milk, whey protein and caseinate. |
Method for production of pectin from palma christi fruit shells / 2415608 Invention relates to food industry, in particular - to a technology for release of pectin from plant raw material. The method envisages fruit shell drying and milling, removal of impurities. Then one degreases the milled fruit shell with acetone during 24 hours. One performs removal of polyphenols, salt - and water-soluble proteins. Then one performs the raw material with drinking water (2-3-times). Then one proceeds with hydrolytic extraction with a 0.3-0.5% solution of citric acid during 120 minutes at a temperature of 85-90°C, duty of water being 1:10. One separates the liquid phase. For pectin substances coagulation acetone is utilised. Then the coagulate is dried and ground. |
Raw material grinding method for production of pectin and juices and device for its implementation / 2415607 Invention relates to a technology and devices for raw material grinding, in particular - to production of pectin and juices and other products in food and chemical industry. The method involves raw material grinding in a disintegrator and subsequent fine grinding whereby pulp, discharged from the disintegrator (1), is directed in the form of a stream through a nozzle (8) onto a barrier (9) with the help of a high-pressure pump (6), stream rate being V≥k·[12σδε/(pd)]0,5 where σ is strength of the cell membrane cellulose part, δ is thickness of the membrane cellulose layers, ε is elongation at rupture, d is the cell radius, p is the intracellular medium density, k is the coefficient that accounts for the difference between theoretical and actual impact parameters equal to 1.3…1.5. The device is designed in the form of a disintegrator (1) rotor drives whereof are designed in the form of active hydraulic turbines (3), on the blades (9) whereof one delivers (through the nozzles (8)) pulp injected by the high-pressure pump (6). One delivers the pulp (6) to the pump inlet in the form of raw material ground in the disintegrator (1) and filtered. The device turbines (3) blades (9) are designed as planes with corrugated or rough working surface. In the second version of the device the blades (9) are fixed immediately on the disintegrator (1) rotors and the nozzles (8) for pulp delivery are built into the disintegrator (1) body. |
Method to produce pectin extract from fruit shells of holy clover / 2414826 Invention relates to food industry. Method provides for drying of fruit shell of holy clover, its grinding down to particle size of 1-4 mm, removal of admixtures, hydrolysis-extraction of pectin substances with 0.3% solution of citric acid at hydraulic module of 1:12. Hydrolysis-extraction is carried out at the temperature of 85-90°C for 120 minutes. Then liquid phase is separated. |
Method of pectin production from black walnut coats / 2414145 Invention relates to food industry. The method envisages fruit coat drying and milling, removal of impurities and degreasing with acetone during 24 hours. Removal of polyphenols is performed with a 5% sodium chloride solution,duty of water being 1:10, at a 75-80°C temperature. Then one undertakes four- or five-time rinsing with potable water. Then one proceeds with hydrolytic extraction with a 0.3-0.5% solution of citric acid during 120 minutes at a temperature of 85-90°C, duty of water being 1:20. For pectin substances coagulation acetone is utilised. Then the coagulant is dried and milled to produce the target product. |
Method for complex synthesis of biologically active substances from alcohol wastes / 2402242 Invention relates to pharmaceutical and alcohol industry and pertains to a method for preparing a complex of biologically active substances (BAS) from alcohol wastes (distillers' spent grains). The method of producing biologically active substances from alcohol wastes is realised by separating distiller's spent grains into a liquid and a solid fraction. The liquid fraction is filtered, evaporated to obtain a concentrate with density of 1.480 g/ml and then treated with acetone in volume ratio concentrate : acetone equal to 1:3. The precipitate is filtered, washed with acetone three times and then dried. The solid phase is extracted through maceration with 1% solution of ammonium oxalate in weight-volume ratio raw material : extract equal to 1:10 at 70°C for 3 hours. The extract is filtered, evaporated to obtain a concentrate with density of 1.480 g/ml and then treated with 95% alcohol in volume ratio concentrate : alcohol equal to 1:2. The precipitate is filtered, washed, dried and the ground. |
Method for pectin gelling property enhancement / 2399301 Invention is related to food industry, namely to technology gelling additives production. In accordance with the method proposed pectin is ground and dissolved, the pectin solution is amidated and a sugar-and-pectin mixture is prepared. Amidation proceeds during 1.5-6 hours at room temperature by way of gaseous ammonia flow through the pectin solution till the share of amides in the total galacuronide content is 60-70 vol. %. |
Method of pectin production / 2395211 Invention refers to food industry, in particular to technology of pectin production. The method involves hydrolysis-extraction of pectin-containing raw materials with nanostructured water in rotary cavitation extractor at the ratio of phases 1: (3-5) and the index of cavitation 2.1-2.5. Then separation of phases is carried out. Microfiltration of liquid phase is carried out with tangential method on membranes with a pore size of about 1.4 microns. Then it is concentrated and subjected to ultrasonic spray drying at a temperature of 50-65°C. |
Method for preparing pectin substance / 2244441 Invention relates to a method for preparing biologically active substances from medicinal vegetable raw, in particular, to preparing pectin substances from wild strawberry leaves (Fragaria vesca L.). Raw is extracted preliminary with hot water at heating to 95oC in the ratio raw : extractant = 1:10 for 1 h to separate water-soluble polysaccharides followed by filtration off. Raw residue is extracted with mixture of 0.5% oxalic acid solution and ammonium oxalate (1:1) in the ratio = 1:20 at 80-85oC for 1 h. The repeated extracted is carried out twice. The vegetable material is separated by filtration and combined extracts are evaporated. Pectin substances are precipitated with 5-fold amount of 96% ethyl alcohol at room temperature. The precipitated dense deposit is filtered off, washed out with 96% ethyl alcohol and dried. Method provides elevating yield of the end product up to 12.5% of vegetable raw mass of wild strawberry leaves. |
Method for manufacturing carbohydrate-containing gelling concentrate for confectionary products / 2246858 The suggested concentrate should be prepared due to pressing the juice out of sugar beet prepared with deodorated carbon dioxide in supracritical state. Residues should undergo hydrolysis-extracting with hydrochloric acid solution obtained directly in the mentioned process at separate supply of water and liquid hydrogen chloride for this stage. Obtained extract without residues should be mixed with sugar beet juice and supplement the blend with liquid ammonia along with an extract obtained due to extracting Mortierella globulifera micromycete biomass. The blend should be concentrated due to vacuum evaporation. The concentrate should be treated with liquid carbon dioxide and supplemented with a solid residue obtained as a result of extracting the biomass of the mentioned micromycete and treated with liquid ammonia. The mixture should be heated up to 60 C, not less. The innovation provides increased output of the target product and improved structure=-forming properties. |
Method for preparing pectin from citrus husks / 2247730 Invention relates to a method for isolating pectin from vegetable raw. Method for preparing pectin from citrus husks involves hydrolysis-extraction of a solid phase and separation of a liquid phase. Before hydrolysis-extraction a solid phase is extracted with ethyl acetate and liquid acetylene successively under the above atmosphere pressure. The second extract is separated without pressure change followed by abrupt dropping pressure over a solid phase up to atmosphere value and feeding a solid phase to hydrolysis-extraction. Invention provides reducing loss of pectin being without deterioration of its organoleptic properties. |
Method for isolating pectin from sunflower heads / 2247731 Invention relates to a method for isolating pectin from the vegetable raw. Method for isolating pectin from sunflower heads involves their milling, denaturation of proteins by heating, hydrolysis-extraction of solid phase, separation of liquid phase and its concentrating and drying. Extraction with dimethylformamide is carried out before hydrolysis-extraction stage followed by extraction with liquid carbon dioxide under above atmosphere pressure. The second extract is separated without change of pressure followed by abrupt drop of pressure over the solid phase up to atmosphere value and feeding the solid phase to hydrolysis-extraction stage. Invention provides improving safety due to exclusion contact of toxic solvent with the end product, reducing time process of hydrolysis-extraction stage and reducing loss of pectin substances. |
Method for preparing pectin from citrus husks / 2247732 Invention relates to a method for preparing pectin from vegetable raw. Method for preparing pectin from citrus husks involves hydrolysis-extraction of a solid phase and separation of a liquid phase. Before hydrolysis-extraction a solid phase is extracted successively with acetone and mixture of liquid acetylene and carbon dioxide taken in the mass ratio acetylene : carbon dioxide from 3:7 to 7:3, respectively, under the above atmosphere pressure. The second extract is separated without the pressure change followed by abrupt dropping pressure over a solid phase to atmosphere value and feeding a solid phase to hydrolysis-extraction. Invention provides reducing loss of pectin being without deterioration of its organoleptic properties. |
Method for preparing pectin from citrus husks / 2247733 Invention relates to a method for isolating pectin from vegetable raw. Method for preparing pectin from citrus husks involves hydrolysis-extraction of a solid phase and separation of a liquid phase. Before hydrolysis-extraction a solid phase is extracted with dimethylformamide and liquid acetylene successively under the above atmosphere pressure. The second extract is separated without pressure change followed by abrupt dropping pressure over a solid phase up to atmosphere value and feeding a solid phase to hydrolysis-extraction. Invention provides reducing loss of pectin being without deterioration of its organoleptic properties. |
Method for preparing pectin from citrus husks / 2247734 Invention relates to a method for isolating pectin from vegetable raw. Method for isolating pectin from citrus husks involves hydrolysis-extraction of a solid phase and separation of a liquid phase. Before hydrolysis-extraction a solid phase is extracted with dimethylformamide and liquid carbon dioxide successively under the above atmosphere pressure. The second extract is separated without the pressure change followed by abrupt dropping pressure over a solid phase up to atmosphere value and feeding a solid phase to hydrolysis-extraction. Invention provides reducing loss of pectin being without deterioration of its organoleptic properties. |
Method for preparing pectin from citrus husks / 2247735 Invention relates to a method for isolating pectin from vegetable raw. Method for preparing pectin from citrus husks involves hydrolysis-extraction of a solid phase and separation of a liquid phase. Before hydrolysis-extraction a solid phase is extracted with acetone and liquid carbon dioxide successively under the above atmosphere pressure. The second extract is separated without pressure change followed by abrupt dropping pressure over a solid phase up to atmosphere value and feeding a solid phase to hydrolysis-extraction. Invention provides reducing loss of pectin being without deterioration of its organoleptic properties. |
Method for isolating pectin from citrus husks / 2247736 Invention relates to a method for preparing pectin extract from vegetable raw. Method involves the successive extraction of citrus husks with acetone. Then after separation of extract a solid phase is extracted with a mixture of liquid acetylene and carbon dioxide taken in mass ratio from 3:7 to 7:3. Then hydrolysis-extraction of a solid phase is carried out and a liquid phase is separated after termination of the hydrolysis-extraction process. Method provides reducing loss of pectin. |
Method for preparing pectin / 2247737 Invention relates to a method for isolating pectin from vegetable raw. Method for preparing pectin involves milling and mixing sunflower heads and citrus husks, hydrolysis-extraction of mixture, separation of a liquid phase and isolation of the end product from its. Before mixing sunflower heads and citrus husks are extracted with ethyl acetate and liquid carbon dioxide separately and successively under the above atmosphere pressure. The second extract is separated without pressure change followed by dropping pressure over a solid phase up to atmosphere value and feeding a solid phase to hydrolysis-extraction. Invention provides enhancing quality of the end product due to elimination of undesirable taste and odor and without deterioration of its technological properties and without reducing the specific yield of pectin. |
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