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Method of measuring permittivity of dielectrics

Method of measuring permittivity of dielectrics
IPC classes for russian patent Method of measuring permittivity of dielectrics (RU 2251706):
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FIELD: measuring engineering.

SUBSTANCE: method comprises determining permittivity of petrol. The permittivity of petrol is measured in the identification numbers. The reference points of the liner scale of a measuring instrument are assumed to be the values of the permittivity of chemically pure heptane and toluene. The measurements are performed by submerging the sensor of the measuring instrument into the study petrol. The value of permittivity is determined from the formula proposed.

EFFECT: enhanced accuracy of measuring.

2 cl, 5 app

 

The invention relates to measurement techniques, in particular to a method of measuring the dielectric constant of the dielectric environments, and can be used in electronic and petrochemical industries in the process of measuring and controlling the dielectric constant of the dielectric medium.

As a rule, in the process of measuring the dielectric constant of the dielectric environments, the measurement results are displayed on the display device, printed measuring scale. However, all currently existing scales do not give high accuracy of the measurement of the dielectric constant.

Current methods of measurement of physical quantities and their measurement scale standardized GOST 5365-73. There are also known solutions in the technology of measurement of physical quantities, are protected by copyright certificates No. 1383095 A1 from 09.07.1980, class: G 01 D 13/04 was investigated (2nd column) and No. 1569747 A1 from 19.02.1988, class: G 01 R 27/26.

However, all these methods of measurement do not allow with sufficient accuracy and simplicity to display indicators of the dielectric constant.

As the closest analogue (prototype) of the claimed technical solution is known a method of measuring the dielectric constant of the fluids described in the author's certificate of the USSR No. A from 24.04.1989,, class: G 01 R 27/26).

In the specified way the value of the dielectric permittivity measured by irradiation of the investigated liquid electromagnetic wave with linear polarization through the dielectric prism with obtaining ellipsometric parameters of the reflected wave and then determine the magnitude of the dielectric constant based on linking it with the wavelength corresponding to the minimum ellipticity.

However, this method has significant disadvantages, for example, it is technically difficult, time consuming and, as the above solution does not have the accuracy required in measuring the dielectric constant.

The essence of the method

To measure the dielectric constant of any liquid combustible substances, such as gasoline And 76 - AI 98, take calibration (gastromony) standard. The indices of the dielectric constant of the liquid combustible substances correspond to the indices of the dielectric constant of compounds such as, “heptane” - 1,927; “hexane” - 1,90; “isooctane” - 1,943; “octane” - 1,946; “pentane” - 1,843 etc. to Distinguish and perceive numerical indices of the dielectric constant at the specified value (after 1 there are three numbers) is quite difficult.

For the main group of oil products produced by industry, index permeable dielectric is t ε as a rule, is in the range of 1.8-2.0. Experimentally proved, that the main differences εfor example, for gasoline are in the second, the third sign after a comma, for gastromony, for example, heptane, and other gasoline.

If you measure the gasoline, as a reference it is proposed to use “heptane” ε=1,927, then the accuracy of the measurement should be an order of magnitude above the last decimal place, i.e., the measurement error can reach ±0,0001, and the measurement result is 1,9271-1,9269. This means that the percentage error should not exceed ±0,01%.

Proposed numerical values of the dielectric constant obtained by measuring, for example, hydrocarbon liquids present in conventional units or “identity units” (“And”). Thus, the performance values of the identification numbers derive their dielectric constant.

An example of measuring ε gasoline in the identification And numbers.

Taken at the control point of the linear scale of the instrument (lower and upper point) value ε chemically pure, kostrounova heptane and toluene, which are 1,927 and 2,378 respectively.

Thus:

And=“0” - corresponds to heptane its value ε=1,927 (bottom).

And=“88” - corresponds to toluene E. what about the value ε =2,378 (the top point).

Formula translation of the dielectric constant of identification numbers:

And=195,122 (ε-1,927), where:

195,122 - the number obtained on the basis of experiments.

1,927 value of ε heptane.

Hence: value ε is determined by the formula:

ε=And/195,122+1,927.

The claimed method of measuring the dielectric constant allows hundreds of times to increase the accuracy of measurements. Identification numerical values are more accurate for the record εthey are easily perceived, remembered and compared. Main range of measured values, And ranges from “0” to “100” conventional units or identification units.

The upper reference point is the identification number “100”, which corresponds to a dielectric constant that is determined by the formula:

εmax=100/195,122+1,927=2,4395.

Each petroleum product, such as gasoline, has its own identification number, which allows its identification at all stages of production, transportation, storage and marketing.

The same brand of gasoline produced at different factories have different identification number that allows you to identify the manufacturer of the products. The indicator “identification number” can be used to classify and control the dielectric is of recov: diesel fuels, oils, gases, aqueous solutions, alcohols, etc.

The proposed method allows hundreds of times, almost 200 times, to increase the accuracy of measurements.

All existing devices that are used to measure the dielectric constant, can be transferred for measuring ε identification number.

Below is the analysis of petroleum products on the instrument AAS-2000.

As samples were taken gasoline at different petrol stations in the city of Krasnodar and the Krasnodar territory. Sample analysis was performed in parallel on three devices AES-2000. For each series of tests took the sample of the fuel was mixed and measured in the position of the sensor (measuring head) of the device on the bottom of the tank with the analyzed sample and the weight. The sensor in position on the bottom was put in a glass with a speed of one second and four seconds, to determine the dependence of the differences identification number from the speed measurement. We also made measurements of the index of “And”, but in the position of the sensor on weight.

Similar tests conducted with the same sample of oil after settling samples within thirty minutes. The test results are attached (see table 1-5).

The data obtained indicate that the proposed method of measuring the dielectric permittivity of the dielectric is historical environments allows to determine the dielectric properties of a non-conductive fluid through the indicator “identification number”. In addition, the numerical values of this index can accurately determine the index of the mixture in the analyzed fuel.

1. The method of measuring the dielectric constant of gasoline, which consists in conducting the measurement and subsequent measurement of dielectric permittivity, characterized in that the measured dielectric constant of gasoline in the identification And numbers for reference point linear scale measuring device accept the values of dielectric permeability of chemically pure heptane and toluene, with an identification number And a=0 corresponds to the value of ε=1,927, and identification number And=88 corresponds to the value of ε=2,378, measured by periodically lowering the sensor of the measuring device in the test gas, and the value of the dielectric constant is determined by the formula

ε=And/195,122+1,927, where

ε - the value of dielectric permeability;

And - the identification number shown on the meter scale in the interval starting from 0 to 100;

195,22 - the number obtained experimentally;

1,927 - index dielectric permittivity of heptane.

2. The method according to claim 1, characterized in that the upper reference point is the identification number 100, which corresponds to a dielectric constant that is determined by the formula

εmax=100/195,122+1,927=2,4395.

3. The method according to claim 1, characterized in that the frequency lowering and lifting the sensor of the measuring device in the test gas is 2-4 C.

 

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