RussianPatents.com
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Fire-resistant mixture and multicomponent material for protective coatings of heating elements based on lanthanum chromite made from said mixture. RU patent 2389709. |
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FIELD: chemistry. SUBSTANCE: invention relates to heat-resistant nonmetallic materials and can be used to make effective protective coatings of heating elements based on lanthanum chromite working in an air atmosphere. The invention involves use of a heat-resistant mixture composed of lanthanum chromite, frits from oxide phases and aluminoborosilicate glass with the following ratio of ingredients, in wt %: lanthanum chromite 32-44, frit 43-48, aluminoborosilicate glass 13-20. The frit from oxide phases contains the following components, in wt %: yttrium oxide Y2O3 63-65, aluminium-magnesium spinel MgAl2O4 13-21, lanthanum aluminate LaAl11O18 6-13, mullite Al6Si2O13 6-13, aluminoborosilicate glass SiO2 53-55, CaO 18-20, Al2O3 13-15, B2O3 9-11, MgO 2-4. The multicomponent material for protective coatings obtained from the mixture contains crystalline phases and a glass phase in the following ratio, in wt %: LaCrO3 29-42, Y2O3 30-31, MgAl2O4 6-8, LaAl11O18 3-5, Al6Si2O13 3-5, aluminoborosilicate glass phase 16-22. EFFECT: fire-resistant mixture and multicomponent material provides strong adhesion of protective coatings to the surface of heating elements based on lanthanum chromite, prevention of crack formation and flaking of protective coatings during thermal cycles, longer life of heating elements with the protective coating. 2 cl, 7 ex, 4 tbl, 1 dwg
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Protective coat / 2383514 Protective coat contains liquid potassium glass and powdery fillers, at the following ratio of components in weight parts: liquid potassium glass - 100-150, silicon carbide - 100-200, graphite - 1-12, sodium fluorsilicate - 0-12. |
Method for manufacturing of composite material / 2379268 In manufacturing of a composite material, a carbon-base filling cloth is used as a material blank impregnated with a compound of liquid Bakelite 100 weight fractions, isopropyl alcohol 54-100 weight fractions, tetraethoxysilane 44-160 weight fractions and water 7-32 weight fractions. Thereafter drying, consolidation and thermal processing at temperature 1800-2000°C with formation of silicon carbide follow. |
Method of preparing super-hard coated abrasive / 2378231 Described is a method of preparing a super-hard coated abrasive, specifically a coated abrasive based on diamond or cubic born nitride (cBN). When realising this method, an inner layer of an element which is capable of (individually or combined with other elements) forming carbides, nitrides or borides is deposited onto the surface(s) of abrasive material at the first stage through a hot coating method. The hot coating method is selected from a group a group comprising a method of depositing from gaseous phase via thermal decomposition of metal halides, a method of chemical deposition from vapour phase and a thermal diffusion coating method. Vanadium, molybdenum, tantalum, indium, zirconium, niobium, tungsten, aluminium, boron and silicon are usually used for depositing the inner layer. Through reactive sputtering using a reactive gas, the inner layer is coated with at least one outer layer made from material selected from a group comprising metal carbides, metal nitrides, metal borides, metal oxides and carbonitrides, boronitrides and borocarbonitrides of metals, for example carbide or nitride of titanium, silicon or aluminium. |
Composition for manufacturing carbon silicon-carbide material / 2375333 Siliconising composition includes the following components, parts by weight: liquid bakelite BZh3 - 100, isopropyl alcohol - 67-100, tetraethoxysilane - 53-160, water - 11-32. |
Composition for thermal barrier, machine unit from superalloy with coating containing such composition, ceramic coating and method of coating obtaining / 2365565 Invention relates to composition of ceramic thermal barrier, used in machine units from superalloy. Composition contains base from zirconium oxide, at least one trivalent oxide from group containing erbium oxide, europium oxide, praseodymium oxide, terbium oxide, holmium oxide and their mixtures, allowing to stabilise zirconium oxide and optimally reduce zirconium oxide heat conductivity, and at least one pentavalent oxide from group: niobium oxide, tantalum oxide or their mixture, allowing to reduce number of oxygen vacancies in such way that it was in fact equal to number of oxygen vacancies in partially stabilised zirconium oxide. Said trivalent oxide is present in molar concentration created by the first part, allowing partial stabilisation of zirconium oxide, and by the second part, which introduces point defects into grid, said pentavalent oxide being present in molar concentration equal to molar concentration of said second part of trivalent oxide. |
Method of ceramic item engobing / 2356874 Invention concerns ceramic item production, mainly of ornamental purpose. Method of ceramic item engobing involves application of engobing coating onto twisted textile fiber with further fiber positioning fiber onto an item surface, drying and glazing. Twisted textile fiber can be divided in lengthwise sections coated with angobe layer of different colours. Engobing utilises twisted organic textile fiber burned out later during glazing. |
Method for processing of fire-resistant products / 2356873 Invention is related to production of fire-resistant products and may be used in aviation and rocket engineering. Technical result is achieved by layerwise saturation of refractory material surface with carbon by means of fullerene solution impregnation in organic dissolvent. Product is placed above heating element so that temperature of saturated surface does not exceed 60-65°C, fullerene solution is supplied in organic dissolvent onto product surface so that complete surface is wetted, and impregnation is carried out for 30-45 minutes. |
Method of manufacturing of pottery ware and ceramic product / 2348599 Process of decoration of ceramic ware may be used in creation of various ceramic products possessing decorative and decorative - utilitarian function. Method of manufacturing of pottery wares includes product forming out of loamy raw material, preliminary drying reaching leather - solid state, decoration with colored engobes, final drying and burning. During process of decoration spot of application of background engobe is restricted by at least one local spot, formed by one closed circuit of cutting, at least, one layer of background engobe of the color contrast to that of the foundation is applied on the foundation; there after the product is dried and texturised by cutting of the background layer with applied engobes uncovering foundation of the product; there after received decorative elements are painted with multicolored engobes and refreshed by additional cutting getting as a result corresponding ceramic product. Cutting is conducted with V-shaped profile and/or V-shaped profile and undercutting and/or rounding - off of the profile uncovering foundation of the product. |
Carbon material coated in tantalum carbide and method of obtaining it / 2337899 Invention pertains to carbon material coated in tantalum carbide, which can be used as a component part of a device for making monocrystals of binary semiconductor compounds. According to the invention, carbon material consists of carbon substrate and film, formed indirectly or through intermediate layer on the above mentioned carbon substrate. The film is 10-100 mcm thick and consists of several tightly packed monocrystals of tantalum carbide. On an X-ray diffraction pattern of the film, the diffraction intensity of plane (220) of tantalum carbide has a maximum level. The above mentioned diffraction intensity is not less than 4 times more than the intensity of the second largest diffraction intensity. The method of obtaining the above mentioned material involves forming on the carbon substrate, film of tantalum carbide using CVD method and thermal processing at 1600-2400°C. |
Method of obtaining of cordierite ceramic pigment / 2332366 Invention relates to obtaining heat-resistant ceramic pigments for colouring ceramic masses and glazes, as well as for obtaining under-glaze and over-glaze ceramic paints. Method consists in the following: charge containing mixture of talc, kaolin and technical alumina, providing stehiometric composition of cordierite, is mixed with solution of chromophore in concentration 4.0-15.6 g-ion/100 g of solution according to volume ratio "mineral powder : chromophore solution" 1:1 - 1:4 and boiled for 30-60 minutes. Then sediment is separated from solution, dried and burned at temperature 1100-1200°C. Boiling of charge ensures more equal distribution of colouring salt throughout the volume of mineral powder mixture before synthesis, which facilitates process of embedding of colouring ions into crystalline structure of cordierite during burning and makes it possible to increase brightness of pigments. Obtained pigments have bright-blue, beige, sand, green, red-brown colour. |
Method of manufacturing yttrium oxide-based transparent ceramics and inorganic scintillator based thereon / 2255071 Invention relates to scintillation technics designed for registration of α-, β-, γ- and X-emissions for use in radiotechnology, dosimetry, in nuclear research, etc. Transparent ceramics is manufactured by adding lithium carbonate in amount 0.7-1.0% to starting yttrium oxide powder followed by hot pressing at 34.0-35.9 MPa and 1200-1300°C. Inorganic scintillator comprises working medium containing forward surface with port to receive ionizing α-, β-, γ- and X-emissions, oppositely located back surface, and two side surfaces. Working medium is made from yttrium oxide-based transparent ceramics obtained as above. |
Method of manufacturing yttrium oxide-based transparent ceramics and inorganic scintillator based thereon / 2255071 Invention relates to scintillation technics designed for registration of α-, β-, γ- and X-emissions for use in radiotechnology, dosimetry, in nuclear research, etc. Transparent ceramics is manufactured by adding lithium carbonate in amount 0.7-1.0% to starting yttrium oxide powder followed by hot pressing at 34.0-35.9 MPa and 1200-1300°C. Inorganic scintillator comprises working medium containing forward surface with port to receive ionizing α-, β-, γ- and X-emissions, oppositely located back surface, and two side surfaces. Working medium is made from yttrium oxide-based transparent ceramics obtained as above. |
Fire-resistant mixture and multicomponent material for protective coatings of heating elements based on lanthanum chromite made from said mixture / 2389709 Invention relates to heat-resistant nonmetallic materials and can be used to make effective protective coatings of heating elements based on lanthanum chromite working in an air atmosphere. The invention involves use of a heat-resistant mixture composed of lanthanum chromite, frits from oxide phases and aluminoborosilicate glass with the following ratio of ingredients, in wt %: lanthanum chromite 32-44, frit 43-48, aluminoborosilicate glass 13-20. The frit from oxide phases contains the following components, in wt %: yttrium oxide Y2O3 63-65, aluminium-magnesium spinel MgAl2O4 13-21, lanthanum aluminate LaAl11O18 6-13, mullite Al6Si2O13 6-13, aluminoborosilicate glass SiO2 53-55, CaO 18-20, Al2O3 13-15, B2O3 9-11, MgO 2-4. The multicomponent material for protective coatings obtained from the mixture contains crystalline phases and a glass phase in the following ratio, in wt %: LaCrO3 29-42, Y2O3 30-31, MgAl2O4 6-8, LaAl11O18 3-5, Al6Si2O13 3-5, aluminoborosilicate glass phase 16-22. |
Transparent ceramic material and method of obtaining it / 2473514 Invention relates to field of obtaining ceramics. Claimed material contains matrix, made in form of solid solution of scandium oxide in yttrium oxide with composition Y1-xScxO1.5, where x=0.25-0.35, and filler, made in form of solid solution of scandium oxide in yttrium-aluminium garnet with composition Y3-3zAl5-5zSc8zO12, where z=0.20-0.45, with material containing matrix in amount 80-90 wt % and filler in amount 20-10 wt %. Described is method of material obtaining, which includes mixing of preliminarily obtained matrix with preliminarily obtained filler, mixture formation and thermal processing. |
Thermostatic coating composition / 2248954 Claimed composition contains (mass %): potassium metasilicate with module of at least 4.5 and density of 1.185-1.195 g/ml 24-30; distillated water 23-37; and modified zirconium(IV) oxide of high purity as a pigment. Coating composition of present invention is useful in passive thermostatic systems for spacecrafts. |
High-temperature coating / 2253638 Invention is related to aircraft industry and intended to use for protection of nonmetallic materials based on silicon carbide matrix and carbon fiber filler against oxidation. High-temperature coating is composed of, wt %: silicon 4-6, boron 2-4m hafnium oxide 60-65, hafnium boride 6-10 and, additionally, hafnium silicides 7-10 and silicon boride 2-4. Resulting carbon-silicon composites are resistant to temperature 2000°C. |
Heat-resistant coating / 2255076 Invention relates to coatings to protect parts of exhaust system of gliders made from heat-resistant alloys and corrosion-resistant steels against high-temperature gas corrosion under operation at temperatures up to 600°C. Coating contains, wt %: SiO2 20.0-36.5, B2O3 4.0-5.0, Al2O3 5.0-6.0, BaO 5.0-6.0, CaO 2.0-4.0, MgO 0.5-1.5, TiO2 1.5-2.5, Cr2O3 15.0-17.0, Na2O 0.6-0.7, P2O5 0.5-1.5, sodium liquid glass 23.0-27.0, and mineral silica-based complex compound 5.0-6.0 composed of, wt %: SiO2 56.25-58.05, Al2O3 34.3-35.1, CaO 1.0-1.2, MgO 1.0-1.1, K2O 2.5-2.6, Na2O 0.6-0.7, TiO2 1.6-1.8, SO3 0.15-0.25, Fe2O3 0.8-1.0, or, instead of SiO2 56.25-58.05, SiO2 35.25-40.05 and SiB4 18.0-21.0. Reliability of operation with thus coated parts is increased by a factor of 1.5-2. |
Engobe / 2257364 The invention is pertaining to the field building industry; production of ceramic building materials, for example, it may be used in production of the color ceramic bricks applied for an external lining of buildings, facilities and formation of interiors. The engobe for a facing ceramic bricks contains in its composition (in mass %): a wollastonite concentrate - 31-35, a colorless transparent glassbats - 35-40, burnt gault or burnt clear gault - the rest. The engobe is prepared using a slip process by a wet grist in a ball mill. The acicular form of wollastonite crystals provides a good hiding of an angobe coating, and in a combination with glass bats - an adhesive strength of the coating. Blockading of the open pores on the face surface of an item due to a densely sintered angobe layer results in a decrease of the general hydraulic conductivity of the items and at a sufficient cohesive strength of a decorative layer with the ceramic basis improves frost resistance of the decorated lining ceramics. The high chemical purity of the wollastonite concentrate and utilization of colorless transparent glass bats (with the contents of staining oxides of no more than 0.20 %) increases the coating whiteness and improve the decorative properties of the angobed items. The necessary color palette of the coating depends on the choice of a ceramic pigment. The technical problem of the invention is to increase the strength of adhesion with the ceramic base, to improve whiteness and frost resistance of the items. |
Method of passivation of contact surface of refractory reservoir made from mullite and slip used for realization of this method / 2266880 Proposed method includes application of slip on contact surface; slip contains 50-70 mass-% of aluminum oxide powder Al2O3 and 30-50 mass-% of binder which contains 50-60 mass-% of aluminum chloride AlCl3 dissolved in 40-50 mass-% of water. Then reservoir is dried and roasted in oxidizing atmosphere at temperature of 1450-15500°C for at least 20 min. In some cases, use is made of slip containing water-soluble organic dye. Used as organic dye is methylene blue at total content of 0.1-0.5 mass-%. Specification gives description of slip used for passivation of contact surface of refractory reservoir. Proposed method makes it possible to form absolutely inert coat on contact surfaces of ceramic reservoirs relative to alloys of titanium coat. |
Ceramic filter element manufacturing process / 2274622 Invention relates to manufacturing filter element suited to filter pulps and effluents from galvanic shops. Preliminarily, magnesium montmorillonite cake is prepared at temperatures sufficient to remove gas-forming components, which cake is then ground to particle size not less than pore size in permeable surface of substrate. Mix is further prepared from naturally occurring magnesium montmorillonite and cake, content of the latter in mix being within a range of 30 to 70%. Thereafter, aqueous suspension is prepared comprising uniform fused corundum and above mix in solid phase. This suspension is used to deposit membrane material components. Subsequent heat treatment is conducted with isothermal exposure periods at temperatures sufficient to remove physically adsorbed and crystallization moisture, to cause residual gas emission, and melting of fusible components of membrane layer. Cooling to 400°C is conducted under forced air circulation conditions and, below 400°C, under natural heat convection conditions. |
Porous aluminum-wetting ceramic material / 2281987 Claimed material contains open-porous or gauze ceramic structure, wherein surface of said structure under using is exposed by melted aluminum and wetted therewith. Structure is made of ceramic material which is inert and resistant to melted aluminum such as alumina, and aluminum-wetted material including metal oxide and/or partially oxidized metal such as manganese, cobalt, nickel, copper or zinc, which is capable to interact with melted aluminum to produce surface layer, containing alumina, aluminum and metal, obtained from metal oxide and/or partially oxidized metal. Ceramic structure includes coating from aluminum-wetted material carried on inert and resistant material or comprises mixture of inert and resistant material and aluminum-wetted ceramic material. |
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