Toilet soap with peeling and moistening properties
IPC classes for russian patent Toilet soap with peeling and moistening properties (RU 2311450): C11D3/14 - Pigments; Fillers; Abrasives C11D17 - Detergent materials or soaps characterised by their shape or physical properties (shaping soap C11D0013140000) A61K8/18 - PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES (devices or methods specially adapted for bringing pharmaceutical products into particular physical or administering forms A61J0003000000; chemical aspects of, or use of materials for deodorisation of air, for disinfection or sterilisation, or for bandages, dressings, absorbent pads or surgical articles A61L) Another patents in same IPC classes: Cleansing paste to clean solid surface and cleansing paste production line / 2294358 Cleansing paste suitable to clean and sanify enamel and metallic kitchen dishes, sanitary ware such as washing stands, bathes, lavatory pans, gas burners and the like, marble and ceramic surfaces contains, wt %: sulfonol 3-5, soda ash 10-20, odorant 0.4-1.2, mineral sludge coming as waste from production of protein-vitamin concentrate 52-58, brine of naturally occurring bischofite mineral MgCl2·6h2O (density 1.2-1.3 t/m3) 4-6, and water the balance. Cleansing paste production line comprises sulfonol, soda ash, and odorant supply tanks, transportation means, mixer, vibrator for delivering finished produce, off-line and in-line tanks for finished produce, screw dispensing mechanism, finished produce packaging means, and conveyor for delivering packaged cleansing paste. The line is provided with receiving bin for above mineral sludge, drier, intermediate bin for dried sludge, crusher, sieve classifier, tanks for standard and non-standard sludge, cyclone, fan, hose filter to collect dust fraction of sludge, and sliding shutter. Upstream of mixer, bischofite brine and water tanks are disposed. Solid surface cleaning composition and cleaning process / 2292386 Invention relates to liquid compositions for cleaning solid surfaces and is proved in the form of clear liquid gel with abrasive component and includes one or several cleaning surfactants, abrasive particles, thickening agent and, if necessary, optional components. Abrasive particles dispersed in liquid gel are macroscopic with average particle size between 0.5 and 2.5 mm, all particles having particle size deviation limits ±70% from average particle size. Liquid abrasion detergent compositions / 2265044 Water alkaline abrasion detergent composition comprises, in mass %, 55-80 of abrasion agent, 0.15-0.40 of anion polymer, 0-0.4 of surface active agent and does not comprise thickening clays or thickening silicon dioxide. The detergent compositions can be ready for use or concentrated with at least 55% in mass of abrasion agent, which a consumer can be diluted up to the product ready for use without loss of long-term stability. The composition is allowed to be packed or canned. Solid dispersed abrasive compositions and a method of production of liquid abrasive clearing compositions / 2256699 The invention is pertaining to the field of utilization of solid dispersed abrasive compositions for clearing solid surfaces. The dry composition contains a solid material abrasive and a suspending system eligible for production of a stable suspension at mixing with a liquid medium. It is preferable, that the dry composition should contain at least 65 % of solid abrasive and at least 0.1 % of a suspending system. The suitable suspending systems are based on a surfactant or a mixture of surfactants, which are capable to form a laminated micellar phase after mixing with a liquid medium, or on the basis of polymeric infilling systems. A preferential liquid medium is water. The dry abrasive composition is easily flowing and is easily dispersed in water by a consumer with formation of a liquid clearing composition ready for use. Cleaner / 2235124 The invention relates to the field of household chemicals, namely, powdered tools for sanitary purposes, which can be used to remove dirt from hard surfaces Cleaner / 2221846 The invention relates to cleaners for cleaning household appliances and can be used independently for cleaning hard surfaces: metal containers, Cutlery, window glass, pottery, porcelain, sinks, toilets, and in complex detergents for cleaning industrial equipment Detergent for cleaning metal surfaces / 2216581 The invention relates to the technical detergents designed to clean metal surfaces of residual oil and solids, and can be used when cleaning tanks at refineries and rail ways Composition for cleaning / 2199581 The invention relates to household chemicals, namely thickened tools designed for cleaning hard surface household items, and can be used for cleaning plastics, enamel, tiles, porcelain, faience, glass, metal Cleanser (options) / 2199580 The invention relates to hygiene products and can be used in the manufacture of toothpaste, soap industry, as well as the removal of food stains, greasy and oily films The method of cleaning vehicles, solution-based fibrous material / 2118994 The invention relates to a method of cleaning vehicles, which consists in spraying the vehicle alkaline solution washing composition in a mixture with an aqueous solution of a derivative of cellulose Liquid soap / 2309981 Claimed soap contains potassium carbonate, water, gel-wax soap-waste precipitate, pigment and perfume flavor, Said gel-wax soap-waste precipitate is obtained by sequential treatment of hydrated vegetable oil at 15-35°C with 6-8 % citric acid aqueous solution in amount of 0.5-1.5 % based on oil mass, sodium silicate aqueous solution with density of 1.05-1.15 g/cm3 in amount of 0.5-2.0 % based on oil mass, and sodium silicate aqueous solution with density of 1.20-1.35 g/cm3 in amount of 0.5-4.0 % based on oil mass, exposing of obtained mixture to produce gel-wax soap-waste precipitate followed by isolation thereof from treated oil. All component are used in specific component ratio. Liquid soap / 2309980 Claimed soap contains potassium carbonate, water, phospholipid-gel-wax precipitate, pigment and perfume flavor, Said phospholipid-gel-wax precipitate is obtained by sequential treatment of non-refined vegetable oil at 15-35°C with 3-5 % sodium chloride aqueous solution in amount of 1.0-2.0 % based on oil mass, 6-8 % citric acid aqueous solution in amount of 0.5-1.5 % based on oil mass, and sodium silicate aqueous solution with density of 1.05-1.35 g/cm3 in amount of 0.5-2.0 % based on oil mass, exposing of obtained mixture to produce phospholipid-gel-wax precipitate followed by isolation thereof from treated oil. Lump detergent and a method for manufacture thereof / 2303053 Invention relates to solid molded detergent compositions for cleaning hard surfaces, washing of textiles, or for personal hygiene. Cleaning agent contains 5 to 95% active detergent, 0 to 90% inorganic substance particles or other common ingredients, and at least 5% water. Outside surface of cleaning agent is covered by at least one polymer film formed by radiation hardening of polymer composition capable of being hardened under irradiation. Molded detergent and a method for manufacture thereof / 2303052 Cleaning agent contains 5 to 95% active detergent, 0 to 90% inorganic substance particles or other conventional components, while outside surfaces of agent are closed by protection coating in the form of film having thickness between 5 and 1000 μm and at least one side of cleaner is uncoated. Film is prepared from one or more materials with melting points above 30°C. Coating materials are essentially water-insoluble and water-resistant, are adhered to outside surface of cleaner, and are capable or being removed in time of use. These materials are selected from: (a) naturally occurring or modified natural polymers with water vapor permeability factors below 5000x10-13 [cm3][cm]/[cm2]sec[Pa] and (b) synthetic polymers with water vapor permeability factors below 1000 x10-13 [cm3][cm]/[cm2]sec[Pa], where cm3 relates to volume at 273.15K and pressure 1.013x105 Pa. Advantageously, coating material is a polymer material capable of being polymerized or hardened under the action of heating, ultraviolet, and electron beam irradiation. Cake of cosmetic soap containing latent acidifier (variants) / 2297445 Claimed cake of soap includes fat acid-based soap, anionic surfactant other than soap, latent acidifier, and water in specific component ratio. Acidifier is selected from organic or inorganic compounds or mixtures thereof, or complexes which releases no gas under pH alteration. Moreover acidifier is used in amount effective to produce delta-pH in aqueous suspension more 0.5. Bar of detergent containing anionic surfactant, soap, hydroxyacid salt, and filler / 2294960 Claimed bar of soap contains 10-50 mass % of anionic surfactant; 5-30 mass % of fat acid-based soap; 2-20 % of hydroxyacid salt, and 1-15 mass % of water. As hydroxyacid salt substances of general formula (Ra)(Rb)C(OH)COOM are used, wherein Ra and Rb represent H, F, Cl, Br, alkyl, aralkyl, or aryl groups of saturated or unsaturated, isomeric or non-isomeric, linear or branched, chain or cyclic form containing from 1 to 25 carbon atoms, or OH, CHO, COOH and C1-C9-alkoxy group; M represents organic base or inorganic alkali. Bar of soap is extruded at the rate of at least 150 g/min in laboratory scale extruder. Bar of soap also contains calcite filler wherein ratio of calcite filler and hydroxyacid salt is 0.75:1-2:1 or more. Improved detergent bar and production process / 2294359 Clear soap bar with summary fat substance content 30 to 60% based on the weight of soap, wherein 1 to 15% relates to 12-hydroxystearic acid and precursor thereof and 20 to 50% to at least one polyatomic alcohol, the rest being water. Fabrication of this soap comprises mixing above-listed components, neutralizing resulting mixture with alkali, cooling it, and pouring it into mold followed by ripening over period of time up to 4 weeks. Easily extrudable soap blocks containing alpha-hydroxyacid salts / 2290431 A soap block composition based on fatty acids comprises soaps, α-hydroxyacid salts, monoglyceride, free fatty acid and water. The amount of components of monoglyceride and free fatty acid must comprise separately or in common 3 wt.-% of the composition. The composition can be extruded in the rate 25 blocks per an hour or above. Invention provides preparing the stable a liquid-crystalline phase with retention of properties of the good extrudability. Disposable cleansing article "panchekhi" (variations) / 2281321 Invention provides disposable cleansing article including water-soluble carrier, on which surfactant no.1 is disposed in the form of distinct point-profiled members monolithically linked to carrier and containing differently-shaped bulky cleansing particles monolithically linked to carrier and to each other by means of binder. The latter is water-soluble surfactant no.2 whose dissolution rate in water is below than that of surfactant no.1, while bulky cleansing particles are made from water-soluble material with lower dissolution rate than that of carrier. Cleansing article is bulky and porous with open-cell structure. Improved detergent composition / 2278896 Invention relates to the detergent composition molded by pouring from the melt. The composition comprises less 30% of solid substances and shows the fluidity limit value above 75 kPa in the range of temperatures from 20°C to 40°C and comprises the following components, wt.-%: soap based on saturated fatty acids and comprising one or some salts of (C6-C24)-fatty acids, 2-50; non-soap detergent, 2-40; water, 30-80, and optionally one or some liquid useful agents. The composition has no the pure lyotropic mesomorphic phase in the range of temperatures 20-100°C, and composition forms isotropic liquid phase or dispersion of lyotropic mesomorphic phase in the continuum of isotropic liquid in the range of temperature from 40°C to 100°C. The composition comprises less 5 wt.-% of alcohols, propylene glycol and other polyols and less 1 wt.-% of insalting electrolytes. Method for preparing the solid composition comprises preparing the melt of the detergent composition, pouring melt into form suitable for preparing the required configuration and cooling of the form or its abandonment for cooling. Invention provides enhancing hardness and improvement of consumers' properties. Method for treating atherosclerosis / 2311209 The innovation in question deals with carrying out combined intravenous and external laserotherapy in combination with complex medicinal impact upon the body. Additionally, it is important to fulfill monitor intestinal emptying, daily, about 6-8 procedures/course. External laserotherapy should be carried out onto corporal and auricular points. Medicinal therapy deals with introducing T-activin immunomodulators intramuscularly at the dosage of 100 mcg/d and Halavit at the dosage of 100 mg/d, about 10-20 procedures/course. It is important to apply Aciclovir at the dosage of 1 g/d, therapy course corresponds to 14. The intake of Eiconol in capsules at the dosage of 6-9/d, copper derivatives of chlorophyll at the dosage of 0.1g/d and food additive sodium alginate at the dosage of 4 g/d should be carried out during the whole therapy course. Intravenous and external laserotherapy should be fulfilled at about 8-10 procedures/course. The innovation normalizes cellular and humoral immunity, prolongs the aftereffects of therapy conducted and decreases the number of its complications.	FIELD: cosmetic industry. SUBSTANCE: composition of soft toilet soap contains 20-60 mass % of one or more synthetic surfactants, 10-50 % of moistening agent and peeling particles, wherein at least 20 % of particles have major axis length from 100 to 600 mum. EFFECT: soap with improved peeling and moistening properties. 17 cl, 9 tbl   The present invention relates to soap, suitable for local use for cleansing the body, such as skin and hair. In particular, it relates to compositions of soap that is mild to the skin and exfoliates the skin. Exfoliating toilet Soaps are well known. However, most of them are very irritating to the skin due to the fact that they are based on soap, have a high content of hard or inefficient otshelushivanie, low levels of moisturizers or some combination of the aforementioned. Some of the soap prior with a high content of soft synthetic detergents surface-active substances ("Sindet") and high levels of moisturizers were described as not necessarily contain exfoliating particles or beads, such as beads of polyoxyethylene (polyethylene), walnut shells, apricot pits, and the like. See, for example, U.S. patent No. 6376441, U.S. patent No. 6342470, U.S. patent No. 6384000 and U.S. patent No. 6074998. Unexpectedly, it was found that mild toilet soap containing one or more synthetic detergents surface-active substances, one or more humectants and otslushival with a specific range of particle sizes, provide the consumer at the same time superior moisture and otshelushit the tion. As shown by various conventional in this field the methods described below, it helps to shed the skin of the consumer looked fresh and healthy, as this removes dull layer of dead skin and at the same time being a deep cleaning, which leads to less clogged pores, and at the same time moisturize skin to minimize irritation and dryness. Not wishing to be bound by the following theories skin care, applicants believe that exfoliation improves skin cleansing, helping to mechanically remove skin dirt and grease. It is also believed that exfoliation helps the process of desquamation. Desquamation is a natural process in which the corneocytes removed from the stratum corneum, which is the top layer of skin cells. The corneocytes are just cells that contain the stratum corneum, and they continuously removed as the skin regenerates. Exfoliation helps to remove scaly of corneocytes, which are ready to be chipped off from the stratum corneum and thereby contribute to obtain a smoother, less flaky skin. Other possible health benefits from exfoliation, in addition to improved removal of particles (flakes) and fat removal, as mentioned above, consist in reducing the number of bacteria on the skin and improving skin blood flow thanks fur the systematic stimulation. It is expected that the soap in accordance with the invention in terms of actual application will show improvement in skin softness, smoothness of the skin and is similar to the perceived customer benefits, such as efficiency peeling, softness, efficiency humidification efficiency of sedimentation, the cleaning efficiency and characteristics such Soaps as abrasion of the skin, etc. as changes from baseline measurements obtained using free Soaps without the compositions of the invention, which is quantified using the test methods described below. Therefore, according to the first aspect, the present invention is free soap with: a) purifying a basis containing from about 20 to 60 wt.% one or more synthetic detergents surface-active substances; b) from about 10 to 50 wt.% the humidifier; c) exfoliating particles, of which at least 25 wt.% have a size, measured along the major axis of the particle, from about 100 microns to about 600 microns. In another aspect of the invention presents soap manufactured by a process comprising the stages: (a) preparing at least one synthetic surfactant, at least one humectant, and at least one otshelushivatsya; (b) efficient when blended the ingredients I stage (a) to form a target pre-mixture at a temperature sufficient for a preliminary mixture was fluid, or at a higher temperature, up until the preliminary mixture becomes almost uniform, and otslushival and a substantial part of at least one or more humidifiers are not included in the preliminary mixture; (c) cooling the resulting product is pre-mixture; (d) optionally, grinding or refining of chilled product pre-mixture to obtain granules; (e) mixing otshelushivatsya with a substantial part of one or more humectants, not added to the product of the pre-mixture obtained in stage (b) or (c), with the formation of exfoliating pre-mixture; (f) mixing exfoliating pre-mixture with the cooled product pre-mixture in the mixing of solids; (g) at least one time cleaning product stage (f); (h) extruding and stamping product in the form of soap. In another aspect of the invention provides a method of simultaneous exfoliation and hydration of the skin, which includes stages: a) preparation of Soaps, including: i) purifying the base containing from about 20 to 60 wt.% one or more synthetic detergents surface-active substances; ii) about the 10 to 50 wt.% the humidifier; iii) exfoliating particles, and at least 25 wt.% particles have a size, measured along the major axis of the particle, from about 100 microns to about 600 microns; b) adding sufficient water to wet the soap and skin; c) applying soap on the skin; (d) rubbing soap skin for a time sufficient to remove dead skin cells and covering the lower layers of the skin at least one humidifier. Another aspect of the invention is a method of providing different levels of exfoliation and hydration at different areas of the body of the consumer, which includes stages: (a) preparation of soap, and the soap contains: 1) cleansing base containing from about 20 to 60 wt.% one or more synthetic detergents surface-active substances; 2) about 10 to 50 wt.% the humidifier; 3) exfoliating particles, and at least 25 wt.% particles have an average size, measured along the major axis of the particle, from about 100 microns to about 600 microns; (b) hydrating soap, body or both; (c) rubbing the soap on selected areas of the skin of the consumer in a period of time sufficient to remove dead skin cells where it is desirable significant exfoliation; (d) adding sufficient water to the soap to obtain a foam; (e) natira the Oia foam selected by the user of the skin, where it is desirable moisture without significant exfoliation, over time, sufficient to cover the lower layers of the skin at least one humectant; (f) and phase (c)-(e) can be carried out by the user in any order. One aspect of the present invention is free soap with: (a) cleansing base, preferably having zeinabou number less than 50, 40, 30 or 25; and purifying the core contains from about 20 to 60 wt.%, preferably from 25 to 55 wt.%, one or more synthetic detergents surface-active substances; (b) about 10 to 50 wt.%; preferably from 20 to 45 wt.% the humidifier; (c) exfoliating particles, of which at least 25 wt.%, preferably at least 50 wt.% particles have an average size, measured along the major axis of the particle, from about 100 microns to about 600 microns; preferably from about 100 to 300 microns and more preferably those where the smallest particle in the above mass fraction is 150 microns. Mainly exfoliating particles may have a hardness less than about 4 units Mohs, preferably less than about 3 units Mohs. Preferably exfoliating particles differ in color from cleansing base. Mostly soap according to the invention has the organoleptic index exfoliate, less than or equal to 10, preferably less than or equal to 5, more preferably less than or equal to 3; according to the test method specified below. Exfoliating particles are preferably present in the soap according to the invention at a concentration of less than about 1 wt.%, preferably less than 0.5 wt.%. Exfoliating particles larger than 400 μm, preferably 300 microns, are mostly at a concentration of less than about 0.25 wt.%, preferably less than approximately 0.05 wt.% and more preferably less than approximately 0.025 wt.%. Exfoliating particles are mainly, but not exclusively, to be selected from polyethylene, microcrystalline wax, ester str (jojoba), amorphous silicon dioxide, talc, tricalciumphosphate or mixtures thereof and the like. Preferably they are selected from polyethylene, microcrystalline wax, ester str or mixtures thereof. Soap according to the invention also contains moisturizers, preferably selected from fatty acids, triglycerides, mineral oil, petrolatum, glycerin, polyethylene glycol or mixtures thereof and the like; more preferably they are selected from fatty acids, triglycerides, and most preferably of stearic acid, sunflower oil, or mixtures thereof. Mostly attitude umlani the El to otshelushivaet lies in the range from about 20:1 to 500:1; preferably from about 100:1 to 500:1. As for pH, soap according to the invention mainly provides a water suspension with a pH of from about 4 to 8, preferably from about 6 to 8 and preferably contains less than about 10 wt.%, more preferably less than about 3 wt.% soluble soap, as defined below. Another aspect of the invention is a soap manufactured by a process comprising the stages: (a) preparing at least one synthetic surfactant, at least one humectant, and at least one otshelushivatsya; (b) mixing stage (a) to obtain preliminary product mixture at a temperature (preferably above 85° (C)sufficient to preliminary mixture remained fluid or above this temperature until it's time until the preliminary mixture becomes homogenous (preferably for from about 30 minutes to 1 hour 30 minutes), and otslushival, optional flavoring and a substantial part of at least one or more humidifiers, are not part of the pre-mixture (preferably the number is not part of the humidifier is less than about 5 wt.% of the composition, preferably less than about 2 wt.% composition); (c) cooling the obtained product is a pre-mixture (preferably using a cooling roll or similar); (d) optionally, grinding or refining of chilled product pre-mixture to obtain granules; (e) mixing otshelushivatsya with a substantial part of one or more humectants, not added to the product of the pre-mixture formed in stage (b) or (c)to obtain exfoliating pre-mixture (the remaining moisturizing component is preferably in liquid form or becomes liquid when heated); (f) mixing exfoliating pre-mixture with the cooled product pre-mixture in the device for mixing solids (preferably a ribbon mixer, a refiner, a stirrer with blades in the form of the letter z, and the like); (g) at least one time cleaning product stage (f); (h) extruding and stamping product in the form of soap. Preferably, if should be added flavoring, stage blend perfumes is carried out either simultaneously with the stage of mixing otshelushivatsya and a moisturizer, or as a separate stage to obtain exfoliating pre-mixture. Another aspect of the invention is a method of simultaneous exfoliation and hydration of the skin, which includes stages: (a) preparation of soap containing i) purifying the basis, preferably is within zeinabou number less than 50, 40, 30 or 25; and purifying the core contains from about 20 to 60 wt.%; preferably from 25 to 55 wt.% one or more synthetic detergents surface-active substances; ii) from about 10 to 50 wt.%; preferably from 20 to 45 wt.% the humidifier; iii) exfoliating particles, of which at least 25 wt.%, preferably at least 50 wt.%, have an average size, measured along the major axis of the particle, from about 100 microns to about 600 microns, preferably from about 100 to 300 microns and more preferably those where the smallest particle in the above mass fraction is 150 microns. b) adding sufficient water to wet the soap and skin; c) applying soap on the skin; (d) rubbing soap skin for a time sufficient to remove dead skin cells and covering the lower layers of the skin at least one humidifier. Another aspect of the invention is a method of providing a variable level of exfoliation and hydration in different parts of the body of the consumer, which includes stages: a) preparation of soap, and the soap contains: i) purifying the basis, preferably having zeinabou number less than 50, 40, 30 or 25; and purifying the core contains from about 20 to 60 wt.%, preferably from 25 to 55 wt.% one or more si is synthetic detergents surface-active substances; ii) from about 10 to 50 wt.%, preferably from 20 to 45 wt.% the humidifier; iii) exfoliating particles, and at least 25 wt.%, preferably at least 50 wt.% particles have an average size, measured along the major axis of the particle, from about 100 microns to about 600 microns, preferably from about 100 to 300 microns and more preferably those where the smallest particle in the above mass fraction is 150 microns. b) hydrating soap, body or both; c) rubbing the soap user selected areas of the skin for a time sufficient to remove dead skin cells where it is desirable significant exfoliation; d) adding a sufficient amount of water in the soap to obtain a foam; e) polishing foam user selected skin areas where it is desirable moisture without substantial exfoliation, over time, sufficient to cover the lower layers of the skin at least one humectant; f) where stage (c)-(e) can be carried out by the user in any order. It is expected that the soap according to the invention in actual conditions of use will find improvement in skin softness, smoothness of the skin and is similar to perceived consumer favorable effects, such as the efficiency of peeling, softness, efficiency is vladenie, the efficiency of sedimentation, the efficiency of purification and is the property of the soap, as the abrasiveness of the skin and so on, changes from the baseline for measurements with free soap without the compositions of the invention as defined quantitatively test methods described below. These skin friendly options can also be expressed quantitatively as the ratio of the response to the soap according to the invention the reaction on the comparative soap. Where, as expected, increasing the favorable effect of Soaps according to the invention exceeds the numerical result from comparative soap, found the ratio is above 1.0 in; that is, 1,02, 1,05, 1,07, 1,1, 1,2, 1,3, 1,4, 1,5, 1,6, 1,7, 1,8, 1,9 or 2.0. Where it is expected that improved the favorable effect of Soaps according to the invention will be below the numerical result for the comparative soap, found value will be less than 1.0; that is, 0,99, 0,98, 0,97, 0,95, 0,93, 0,90, 0,85, 0,80, 0,70, 0,60, 0,50, 0,40, 0,30, 0,20 or 0,10. Below table 1-4 show what is expected of the various properties of soap according to the invention compared with four different comparative Soaps. Test methods that can be used to measure properties are listed below. Table 1< / br> Soap according to the invention compared with the Comparative soap A(1)(a piece of soap with otshelushivatsya) Description Relation to the comparative soap A The softness >1 Hydration >1 The subsidence of the humidifier >1 The softness >1 Smoothness >1 Abrasion of the skin(2) <1 1)Comparative soap A: True Blue Spa: Look Cool Minty Fresh Buffing Bar ® Bath&Body Works containing sodium palmitate, Cocoate sodium, water, glycerin, fragrance, wax str, pentetate pentametre, etidronate tetranitride, oil from the leaves of gaultheria supine (simalube), the oil from the leaves of Menta Piperita (peppermint), titanium dioxide (CI77891), Ultramarines (CI 77007) 2)Higher values indicate worse performance. Table 2< / br> Soap according to the invention compared with the Comparative soap B(3)(soap sindet without otshelushivanie) Description Relation to the Comparative soap B Exfoliation >1 The cleaning efficiency >1 The subsidence of the humidifier =>1 The softness >1 Smoothness >1 Organoleptic exfoliation soap >1 3)For example, a piece of soap Dove® from Unilever, which, as indicated on label, contains isetionate sodium and fatty acids of coconut oil, stearic acid, tallowate sodium, water, isetionate sodium, coconut acid, sodium stearate, cocamidopropylbetaine, Cocoate sodium, flavoring, sodium chloride, titanium dioxide, Terentieva salt EDTA, trinitroethanol and butylacetyl. Table 3< / br> Soap according to the invention compared with the Comparative soap C(4)(soap sindet with otshelushivatsya, in which more than 75 wt.% particles have a size, measured along the major axis, less than 100 microns) Description Relation to the Comparative soap C Exfoliation(5) >1 The cleaning efficiency >1 The subsidence of the humidifier =>1 The softness(5) >1 Smoothness(5) >1 Organoleptic exfoliation soap >1 4)Example D (see below), except that otslushival characterized 75 the AC.% particles, whose size, measured along the major axis, less than 100 microns. 5)Clinical trial and/or trial on consumers (method see below). Table 4< / br> Soap according to the invention compared with the Comparative soap D(6)(soap sindet with otshelushivatsya, in which more than 75 wt.% particles have a size, measured along the major axis, more than 600 microns) Description Relation to the Comparative soap D The subsidence of the humidifier =>1 The softness >1 Smoothness >1 Abrasion of the skin(7) <1 Organoleptic exfoliation soap >1 6)Example D (see below), except that otslushival characterized 75 wt.% particles that have a size, measured along the major axis, more than 600 microns. 7)Higher values mean worse performance. Surfactants are an essential component of the composition of the soap according to the invention. They are compounds having hydrophobic and hydrophilic areas, which affects the reduction of surface tension of aqueous solutions, to the which they are dissolved. Useful surfactants may include anionic, nonionic, amphoteric and cationic surfactants and mixtures thereof. The cleansing composition of the present invention may contain one or more nemylnya anionic detergents (Senderov). Preferably sindey have zeinabou number of 50 or less. Zeinabou number can be measured using the test method described below. Suitable anionic washing-active substances include aliphatic sulfonates, such as sulfonates, primary alkane (e.g., C8-C22), disulfonate primary alkane (e.g., C8-C22), sulfonates C8-C22alkenes, sulfonates C8-C22hydroxyalkyl or sulfonates alkylglycerol ether (AGS); or aromatic sulfonates, such as Las. Anionic substance may also be alkylsulfates (for example, C12-C18alkylsulfates) or sulfate Olkiluoto ether (including sulfates alkylglycerol ether). Among sulfates Olkiluoto ether are those which have the formula RO(CH2CH2O)nSO3M where R is alkyl or alkenyl having from 8 to 18 carbon atoms, preferably from 12 to 18 carbon atoms, n denotes an average value greater than 1.0, more preferably 3, and M is lubritorium cation, such as sodium, potassium, ammonium or substituted ammonium. Preferred laurilefirsulfat ammonium and sodium. Anionic agents can also be selected from alkylsulfonates (including mono - and dialkyl, e.g., C6-C22sulfosuccinates); alkyl - and aculturation, alkyl - and acylcarnitines, sulfoacetate, C8-C22alkylphosphates and phosphates, esters of alkylphosphates and esters of alkoxyalkanols, acollection, C8-C22monoalkylamines and malatov, sulfoacetate, Alkylglucoside and utilizationof and mixtures thereof. Sulfosuccinate can be monoalkylsulfosuccinates formula R4About2CCH2CH(SO3M)CO2M; and amide-IEA-sulfosuccinate formula R4CONHCH2CH2About2CCH2CH(SO3M)CO2M where R4means C8-C22alkyl, and M is solubilizers cation. Sarcosinate usually denoted by the formula R1CON(CH3)CH2CO2M where R1applies to C8-C20alcelam, and M means solubilizers cation. Taurate usually determined by the formula R2CONR3CH2CH2SO3M where R2means C8-C20alkyl, R3means1-C4alkyl, and M is solubilizers cation. In SOS is AB toilet soap according to the invention preferably consists of C 8-C14utilizationin. These esters are prepared by the reaction between isetionate alkali metal with a mixture of aliphatic fatty acids containing from 6 to 12 carbon atoms and an iodine number less than 20. Utilization can be alkoxycarbonyl the isetionate, such as described in U.S. patent No. 5393466, Ilardi et al., entitled "Fatty Acid Esters of Polyalkoxylated isethonic acid; issued February 28, 1995; incorporated into this description by reference. This compound has a General formula where R is an alkyl group containing from 8 to 18 carbon atoms, m denotes an integer from 1 to 4, X and Y are hydrogen or alkyl group containing from 1 to 4 carbon atoms, and M+means a monovalent cation such as sodium, potassium or ammonium. In another embodiment, the toilet soap according to the invention contains less than 5 wt.% any of the following anionic surfactants: alkyl sulphates, alkyl sulphonates, alkylbenzenesulfonates, alkylalkoxysilane, acetamido, arylsulfatase and amides of fatty PolicyKit, individually or in mixture. Preferably contains less than 1 wt.%, more preferably less than 0.1 wt.% these surface-active substances. Toilet soap according to the invention may contain soap, preferably it contains less than prima is but 10.0 wt.% soluble soap, more preferably it contains less than about 5 wt.% soluble soap. The term "soap" is used here in the conventional sense, i.e. salts of alkaline metal or alkanolammonium salts of alkane - or alkemadelaan acids. The cations of sodium, potassium, mono-, di - and triethanolamine or combinations thereof, are acceptable for the purposes of the present invention. In General, sodium, potassium, ammonium, mono-, di - and triethanolamine Soaps of saturated C8-C14alkyl chains and unsaturated fatty acids, preferably having a C8-C22alkyl chains are soluble Soaps. In this invention can be applied to one or more amphoteric surfactants. Such surfactants contain at least one acid group. This may be carboxyl or sulfonylurea group. They include Quaternary nitrogen and thus are Quaternary aminokislotami. Usually they should include alkyl or alkenylphenol group with the number of carbon atoms from 7 to 18. Usually they satisfy the General structural formula: where R1means alkyl or alkenyl containing from 7 to 18 carbon atoms; R2and R3every means independently alkyl, hydroxyalkyl or carboxyethyl with the number of carbon atoms is from 1 to 3; n means 2 to 4; m is 0 or 1; X means alkylene containing from 1 to 3 carbon atoms optionally substituted by hydroxyl, Y represents-CO2- or-SO3-. Suitable amphoteric surfactants in the above General formula include simple betaines of the formula and aminobutane formula where n is 2 or 3. In both formulas, R1, R2and R3previously defined. R1may, in particular, to be a mixture of C12- and14is an alkyl group derived from coconut oil, so at least half, preferably at least three quarters, of the groups R1have 10 to 14 carbon atoms. R2and R3preferred are the stands. Another possibility is that the amphoteric detergent is sulfobetaine formula or where m is 2 or 3, or variants of these formulas, in which -(CH2)3SO3 -replaced by In these formulas, R1, R2and R3the same as discussed previously. Assume that atacamite and diaphaneity also included in the scope of the invention in a possible cvit ariannah and/or amphoteric compounds, which can be used, such as lauroamphoacetate sodium, cocoamphoacetate sodium and mixtures thereof and the like. As part of the soap of the present invention may also be used one or more nonionic surfactants. Non-ionic substances that can be used include in particular the reaction products of compounds having a hydrophobic group and a reactive hydrogen atom, for example aliphatic alcohols, acids, amides or alkyl phenols with acceleratedly, especially ethylene oxide, with one or with propylene oxide. Specific nonionic detergent compounds are the condensation products (C6-C22)alkyl phenols and ethylene oxide, the condensation products of aliphatic (C8-C18) primary or secondary linear or branched alcohols with ethylene oxide, and products obtained by condensation of ethylene oxide with the reaction products of propylene oxide and Ethylenediamine. Other so-called nonionic detergent compounds include the oxides, long chain tertiary amines, oxides, long chain tertiary phosphine and diallylsulfide, and the like. Nonnie substances can also be inorganic salts sugars, amides such as polysaccharides. More precisely, the surfactant may be one of lactobionate described in PA is inthe U.S. No. 5389279, Au et al., entitled "Compositions Comprising Nonionic Glycolipid Surfactants", issued February 14, 1995; the contents of which are included in the description by reference, or it can be one of the amides of sugars described in U.S. patent No. 5009814, Kelkenberg, entitled "Use of N-Poly Hydroxyalkyl Fatty Acid Amides as Thickening Agents for Liquid Aqueous Surfactant Systems", issued April 23, 1991; included in the description by reference. An optional component in the compositions according to the invention is a cationic agent or polymer, feel the skin, such as cationic cellulose. Cationic cellulose is sold Amerchol Corp. (Edison, NJ., USA) in their polymer series Polymer JR™ LR™, as salts of hydroxyethyl cellulose reacted with substituted ammonium-epoxide, referred to in the industry (CTFA) polyquaternium 10. Another type of cationic cellulose includes the polymeric Quaternary ammonium salt and of hydroxyethyl cellulose reacted with substituted lauryldimethylamine the epoxide, referred to in the industry (CTFA) polyquaternium 24. These materials are sold Amerchol Corp. (Edison, NJ., USA) under the trademark Polymer LM-200, and Quaternary ammonium compounds such as the halides alkyldimethylammonium. Private appropriate type polymeric cationic polysaccharide, which can be used is a cationic derivative of the guar gums, such as qualitatsprodukten unifloral (commercially available from Rhone-Poulenc in their series JAGUAR™ ). Examples are JAGUAR C13S, which has a low degree of substitution of cationic groups and high viscosity, JAGUAR C15, having an average degree of substitution and a low viscosity, JAGUAR C17 (high degree of substitution, high viscosity), JAGUAR C16, which hydroxypropyltrimonium cationic garolim derivative with a low content of substitute groups, and also containing cationic groups are Quaternary ammonium, and JAGUAR 162, which is highly transparent, the average viscosity of the guar having a low degree of substitution. Especially preferred cationic polymers are JAGUAR C13S, JAGUAR C15, JAGUAR C17, JAGUAR C16 and JAGUAR C162, especially JAGUAR C13S. Can be applied and other well-known from the prior art cationic agents, skin feel, provided that they are compatible with the formulation of the invention. Other preferred cationic compounds that are suitable for use in the present invention include lidocaine Quaternary ammonium, such as propionate and lactate salt of Quaternary ammonium, and Quaternary ammonium protein hydrolysates silk or wheat, and the like. Many of these compounds can be obtained as amidofunctional amines Mackine™, amidofunctional salts of tertiary amines Mackalene™ and cationic protein hydrolysates Mackpro® from McIntyre Group Ltd. (University Park, IL). In the preferred embodiment, is oblasenia of the invention, includes conditioning agent with gidrolizovannykh proteins, the average molecular weight of the hydrolyzed protein is preferably about 2500. Preferably 90% of the hydrolyzed protein has a molecular weight of from about 1500 to about 3500. In a preferred variant embodiment in soap add MACKPRO™ WWP (i.e. hydrolyzed wheat protein aminodiphenylamine wheat germ) in a concentration of 0.1% (as is). This leads to the concentration of "dry matter" MACKPRO™ WWP™ in the final recipe soap for this variant embodiment, equal to 0.035%of. One or more cationic surfactants may also be used in subspinipes cleansing composition of the invention. Examples of cationic detergents are Quaternary ammonium compounds, such as alkyldimethylammonium. Other suitable surfactants that may be used are described in U.S. patent No. 3723325, Parran Jr., entitled "Detergent Compositions Containing Particle Deposition Enhancing Agents", issued on March 27, 1973; and in the publication "Surface Active Agents and Detergents" (vol I and II) Schwartz, Perry &Berch, both documents are also included in the description by reference. In addition, the composition of the soap according to the invention can include from 0 to 15 wt.% the following optional features: fragrant substances, complexing with the organisations, such as Terentieva salt ethylenediaminetetraacetic acid (EDTA), disodium etidronate or mixture in amounts of from 0.01% to 1%, preferably from 0.01% to 0.05%, and dyes, cloud emulsions and substance, giving pearly luster, such as zinc stearate, magnesium stearate, TiO2, EGMS (ethylenglykolether) or Lytron 621 (styrene and acrylate) and the like. All these components are useful for enhancing the appearance or cosmetic properties of the product. In addition, the composition can include an antimicrobial agent, such as 2-hydroxy-4,2',4'-trichlorodiphenyl ether (DP300); preservatives, such as dimethylhydantoin (Glydant XL1000), parabens, sorbic acid, etc. and the like. The composition may also include atilano or diethanolamide coconut oil as amplifiers foaming; can also with advantage be used heavily ionizing salts such as sodium chloride and sodium sulfate. Antioxidants, such as bottled hydroxytoluene (BHT) and the like, can be used mainly in an amount of about 0.01% or more, if appropriate. Can be used water-retaining agents such as polyhydric alcohols, for example glycerol and propylene glycol, and the like, and polyols, such as glycols, listed below, and the like.
Polyox WSR-205	PEG 14M,
Polyox WSR-N-60K	PEG 45M, or
Polyox WSR-N-750	PEG 7M.

In the present invention can preferably be applied humidifiers, also known as water-retaining agents, and softeners. The softening composition may be the only positive component of the current agent or it can be a mixture of two or more compounds, one of which or all of which may have positive aspects. In addition, the agent benefits can act as a carrier for other components, which are preferably added to the soap according to the invention.

Can be applied hydrophobic emollients, hydrophilic softeners, or their mixture. Preferably the hydrophobic emollients are used in addition to the hydrophilic softener in the composition of the soap according to the invention. If they are present, the hydrophobic softeners, are preferably in a concentration of more than about 10 wt.%, most preferably more than about 20 wt.% of the composition. The term "softener" is defined as a substance that softens or improves elasticity, appearance and youthfulness of the skin (stratum corneum) or by increasing the content of water in it, or by adding or replacing lipids and other the nutrients of the skin; or by both, and keeps it soft, slowing the reduction in the content of water in it.

Useful emollients include the following:

(a) silicone oils and their modifications, such as linear and cyclic polydimethylsiloxane; amino-, alkyl-, alkylaryl and analsilicone oil;

(b) fats and oils including natural fats and oils such as butter str, soybean, sunflower oil, rice bran oil, avocado oil, almond, olive, sesame, peach, castor, coconut, mink oils; cocoa butter; beef tallow, lard; hardened oils obtained by hydrogenation of the aforementioned oils; and synthetic mono-, di - and triglycerides such as myristic acid glycerides and glycerides 2-ethylhexanoic acids;

(c) waxes such as karnovsky, spermaceti, beeswax, lanolin and derivatives thereof;

(d) hydrophobic and hydrophilic plant extracts;

(e) hydrocarbons such as liquid paraffin, vaseline, microcrystalline wax, ceresin, squalene, piers and mineral oil;

(f) higher fatty acids such as lauric, myristic, palmitic, stearic, Bekenova, oleic, linoleic, linolenic, lanolin, ezoterikova, arachidonic acid and polyunsaturated fatty acids (Pufas);

(g) higher alcohols, such as lauric, cetyl, stearyl, about eilonwy, beganovic alcohols, cholesterol and 2-hexyldecanol;

(h) esters, such as tetrachromat, myristylated, catallactic, isopropylmyristate, myristoleate, isopropyl, isopropylacetate, butilstearat, decillia, isostearic cholesterol, glycerylmonostearate, glyceraldehyd, glyceroltrinitrate, alkylated, alkiliruth and alkylated;

(i) essential oils and extracts such as menthol, Jasmine, camphor oil, oil of cypress, orange oil from the peel), oil from rye grains, oleoresin, cinnamon and bergamot oil, oil Japanese Mandarin, airnogo, pine, lavender, Bay, clove oil, oil of thevice Japanese, eucalyptus, lemon oil, oil semechnice, thyme, mint, rose oil, sage oil, sesame, ginger oil, Basil oil, juniper oil, lemongrass, rosemary, rosewood oil, avocado, grape oil, grape seed oil, myrrh, cucumber oil, butter, watercress, calendula oil, oil elderflower, geranium oil, oil of lime blossom, amaranth, oil from algae, oil, Ginkgo, ginseng, carrot, oil, guarana, tea tree, str, comfrey, tolagnaro oil, coconut, neroli, vanilla, oil, green tea extract, peppermint oil marsh, oil aloe in the RA, menthol, cineole, eugenol, citral, citronella oil, borneol, linalool, geraniol, evening primrose oil, camphor, thymol, spilanthol, Penin, limonene and terpenoid oils;

(j) lipids such as cholesterol, ceramides, sucrose esters and pseudoceramides, which is described in the description of European patent No. 556957;

(k) vitamins, minerals, and substances which nourish the skin, such as milk, vitamins A, E and K; alkylether vitamins, including alkalemia esters of vitamin C, magnesium, calcium, copper, zinc and other metallic components;

(l) sunscreen compounds such as octylmethoxycinnamate (Parsol™ MCX) and butylperoxybenzoate (Parsol™ 1789);

(m) phospholipids;

(n) antioxidants, such as alpha hydroxy acid, beta hydroxy acid (Aha);

(o) any mixture of the above components and the like.

The preferred softening, beneficial agents selected from fatty acids, triglyceridemia oils, mineral oils, petrolatum and mixtures thereof. Preferred softeners are fatty acids.

Soap according to the invention contains exfoliating particles, which help to remove dry skin. Without being bound by theory, believe that the degree of exfoliation depends on the size and morphology of the particles and their hardness. Large, rough and solid particles are usually very rude and annoying. Very the scarlet particles, which is very soft, can not serve as an effective otshelushivatsya. Hardness is usually measured on the Mohs scale. The scale of hardness according to the Mohs scale is a method used to measure the ability of one substance to scratch more. The scale comprises, in ascending order of relative hardness, from 1 (mild) to 10 (hardest).

Normal otslushival used in this area include natural minerals such as silica, talc, calcite, pumice, tricalcium phosphate; seeds, such as rice, grain, apricot pits, etc.; crushed shell, such as shell almonds and walnuts; oat flour; polymers, such as beads of polyethylene and polypropylene, flower petals and leaves; balls microcrystalline wax; balls of ester str and the like. These otslushival are used in a wide range of sizes and morphology of the particles covering from micron sizes up to several millimeters.

They also have a range of hardness. Some examples are given in table. 5, below.

Otslushival in the present invention have a particle size that at least 25 wt.% particles (preferably at least 50 wt.%) have the major axis (i.e. the largest size particles of irregular shape or the diameter of a spherical particle) from about 100 to 600 microns; preferably from about 100 to 300 microns, and most preferably such that the smallest particle of this mass fraction has a major axis of more than 150 microns; and the particle otshelushivatsya has a hardness of less than about 4, or preferably less than about 3.

Except for the working and comparative examples, or where otherwise explicitly specified, all numbers in this description indicating amounts of material, should be understood as softened by the word "about".

Examples

The following examples are intended to more fully illustrate the embodiments of the present invention. All parts, percentages and proportions referred to herein and in the appended claims, are mass, unless otherwise specified. Physical test methods described below.

The following toilet soap according to the invention can be prepared according to methods manufacturer is, described below:

Examples A through E(PL. 6A and 6B, 7)

Note:

Minor additives include flavoring, salt, preservatives, dyes and/or pigments, etc.

Examples A through E was as follows:

(a) vigorously stirred at a temperature of above 85°C components listed in the table. 6A and 6B, except otshelushivatsya, odorants and sunflower oil, from 30 minutes to 1 hour and 30 minutes until a homogeneous mixture;

b) rapidly cool the hot mixture components using a cooling roller;

c) granularit the product of stage (b);

d) mixing otslushival and sunflower oil; then mix this mixture otshelushivatsya liquid humidifiers with the product of stage (c) in the mixer with blades z-shaped for receiving exfoliating pre-mixture;

e) mix the perfume and exfoliating pre-mixture in the continuous mixer;

f) once rafinuyut product of stage (e), then ekstragiruyut and molded product in the individual detergents toilet soap.

Depending on the properties melting concrete mixture used can also be manufactured from cast melt the pieces of soap. In this case, all components of soap, including otslushival, mix until smooth and then at a temperature sufficient to keep the mixture fluid, is poured into the form. The mixture is then left to cure in ambient conditions or accelerated cooling (such as freezing and the like).

For harakterizovali Soaps according to the invention and comparison with comparative free Soaps may be applied one or more of the following tests.

a)Test for exfoliation:

Suitable dye, coloring the stratum corneum (e.g., gentian violet), put spots with a diameter of 2-5 cm on the skin (hand/foot or any other part of your body at will) and leave for 5 minutes to obtain a uniformly colored surface skin cells (corneocytes). Then the excess ink wash, rinsing the stain running water at 35°C for 30 seconds, the skin do not RUB.

Then painted designated wash the tested product. For soap adopted with EBUSY way of washing. Spot on skin moisturize, slightly moisten the soap, RUB the soap directly on the stain for 30 seconds (movement forward and backward), rinse within 15-30 seconds under running water at 35°C, the skin is not rubbed and dried careful strokes. Dried for 10 minutes. Strip cleaning from dry flakes (Cuderm® production CuDerm Corporation, Dallas, Texas), is superimposed on the washed spot at uniform pressure for 30 seconds and then removed. The cleaning strip is photographed by the digital camera Kodak DCS 420 lens 105 mm

Snapshot analyzed using the software image analysis Optimas for covered square/full intensity of stained cells (Optimas® comes Media Cybernetics, Silver Springs, MD). Comparing these data with similar information for lepromatosa plot as follows to estimate the number of exfoliation caused by the tested product:

Exfoliation = (size of the stripes painted on naramata plot - area stripes painted on the washed area)/(area of the stripes painted on naramata plot)

Alternative exfoliation can also be evaluated in the test on the consumers as follows.

The test Protocol consists of:

1) selection of approximately 10-20 women in the age group 25-65 of those who used soap DL is improving the condition of skin;

2) the application under test and the comparative products, each in a week; half of the test participants must first apply the test product and the other half must first apply comparative product;

3) at the end of the trial, the participants give their preferences (on a scale from 0 to 5 points) for the property "exfoliation".

The degree of exfoliation is determined by estimations of consumers, on a scale from 0 to 5 points

b)Test for softness:

i)Test the controlled deposition on the forearm (FCAT), clinical methodology test

This controlled test washing similar to the test described Ertel et al. ("A forearm controlled application technique for estimating the relative mildness of personal cleansing products", J. Soc. Cosmet. Chem., 46, 67 (1995)).

Participants report on testing tools applied in the study phase of conditioning, which consists of the application is assigned, commercially available personal wash cleanser for General home use, for a period of up to four days prior to the beginning of the phase of application of the product. In the first day phase deposition product is visual assessment to determine the quality of the subject. Subjects must have indicators of dryness >1.0 and indicators redness >0.5 and not have cuts and abrasions on the test site or nearby, to be included in F. the memory material. Those eligible to participate in the phase of application of the product, and then are instructed, in accordance with which they cease to use the air conditioning and any other means to care for the skin on the inner part of the forearm, with the exception of the tested preparations for cleaning the skin, which are applied during the washing session.

Eligible subjects thus have four (round) of the assessment area with a diameter of 3.0 cm marked on each forearm with safety for skin handles (8 plots). Visual assessment of redness and dryness is carried out directly before the first wash in each session and again in the afternoon on the last day (day 5).

The procedure of cleaning products in the form of soap

1. Both hands are washed at the same time. Test plots treated sequentially, starting from the place nearest to the area of the bend, and ending at the place nearest to the wrist.

2. The areas closest to the bend on the inner part of the forearm with both right and left hands moistened with warm water (90-100°F/32-38°C).

3. Moist soft jaws Masslinn study participants RUB in a circular motion on wet soap around 6 seconds, which will lead to the release of 0.2 g to 0.5 g of the product.

4. Plot wash assigned product within 10 seconds, followed by 90 seconds the second phase retention foam.

5. Then the above procedure (1-4) repeat for each of the test plot. Then the sections are washed (e.g., at a temperature of 35° (C) within fifteen seconds and dried Pat.

6. Upon completion of the entire procedure is repeated as a whole (two wash/session).

For liquid products: the analyst should prepare liquid products just before washing session, dealing from 0.1 g to 0.5 g of the product either directly on the skin or on a moistened sponge Masslinn, or an alternative material for the application. Then use the washing procedure described above.

Evaluation methods

Basic visual assessment made prior to the beginning of the phase of application and after application, immediately before each session of washing, to assess the dryness and redness. The final visual assessment is carried out after noon on the last day.

For the evaluation of the test sites to dryness and redness is rated on a scale from 0 to 6 points table. 8. To hide from the evaluators view of the evaluated product, visual evaluations are conducted in a separate area outside the zone of application of the product.

Reading from devices produced in the first (baseline) and the last day of the study.

The softness of the test is the product is calculated as 1/(average change of dryness towards the end of the study).

In addition to the visual assessment will be conducted instrumental assessment of the treated areas using evaporimetry and measuring the conductivity of the skin, as described in the above link.

ii) Testing spots

48-hour continuous or 14-day cumulative test on the affected spots: In the 48-hour test spots 5-15%solution/slurry of the product is applied to the shoulder/back of the subject using a standard cotton swab. The reaction to a stimulus is recorded for up to 24 hours after removal of stains. In 14-day cumulative test 5-15%solution/slurry of the product is applied repeatedly every 24 hours for 14 days. The irritation is written not later than 24 hours after the removal of a stain.

The softness of the product being tested is estimated as 1/(average redness 24 hours after the last spot removal).

c.Test for moisture:

Each of the external lower part of the legs involved in the test subject is divided into three sections 2.5 2.5 square inch (6,4 6,4 cm) - upper, middle and lower - a total of 6 test sites on the subject. One or two of the sites remain undeveloped and will be included in the randomization products. The technician should handle areas once or twice the intended amount of test substance in 10 seconds. Cleansing products should estates is on the test plots within a maximum of 90 seconds. The parts should be rinsed for 30 seconds each (for example, using a temperature of 35° (C) ensuring that the test substance from one area does not contaminate another area. After rinsing the test plots gently wipe with a paper towel. The application consists of applying up to 5 different test substances at a designated place, one substance at one test site and one or two of the unprocessed area. Staff research performs the following procedure wash:

Test phase: Visual assessment

For the evaluation of the test sites on the dryness will use the scale shown in the table. 9.

Basic visual assessment made prior to the beginning phase of product application and after application, immediately before each of instrumental evaluations to assess the dryness and redness. One trained expert makes all the visual evaluation during the phase of application of the product. The expert examines both the lower part of the leg with the aid of a magnifying lamp with illumination lens 3 diopter and shadowless source fluorescent lighting with circular cooling.

Instrumental assessment

All instrumental evaluations are conducted after a 30-min acclimatization period. Data on humidity and temperature are recorded and will include the ENES in the final report. Instrumental measurements can be made in some or all of the following points in time: 0, 1, 2, 4, 6, 8 and 24 hours after applying product. Tools that should be used with this Protocol include evaporimeter ServoMed with sensors EP1 or EP2, corneometer CM820, hygrometer Skicon Skin with sensor MT-8C and hygrometer. The room temperature is kept between 68°F to 77°F (20°C to 25°C)and relative humidity from 30% to 40%.

Hydration is defined as the average change from baseline (visible dryness or skin hydration).

d)Test subsidence humidifier:

Pre-condition the skin of the subject (hands/feet) not containing humidifier product up to 2 days prior to testing. To assess the level of the humidifier (e.g., fatty acids)present on the skin before applying the product, is the basic extraction. Carry out controlled single application of the product on the skin (hands or feet). For washing RUB soap on the skin for 30 seconds, the foam is left for 90 seconds, rinse for 30 seconds (for example, using a temperature of 35°C), then gently Pat dried. After this section is extracted using a suitable solvent (isopropyl alcohol/methanol 1:1). Extraction is as follows: on the skin put the glass bowl (diameter 3 cm). In whom it is placed 3 ml of solvent and gently stirred with a glass rod for 2 minutes. The solvent is removed by pipette. This stage is repeated with 3 ml of fresh solvent to collect a total of 6 ml of the extract. The extracts will be analyzed by the content of stearic acid/palmitic acid, using either LC/MS or GC/MS, or the like.

e)Check for abrasion of the skin:

Abrasion of the skin is determined by the estimated consumer reactions to abrasion on a scale from 0 to 9 points (0 means no erase, 9 means the abrasion caused by the roller (i.e. a washcloth for the soul, consisting of thin plastic fibers, see also, for example, U.S. patent No. 5650384, in the name of Gordon et al.).

This test is carried out with 50 untrained consumers. They are asked to evaluate the abrasion test product on a scale from 0 to 9 points. Data normalized to response on the soap without otshelushivatsya, which is assigned zero points, and to the roller, which is assigned 9 points. The test products are applied in place of the bend of the forearm by wetting the soap and friction movements forward and back 10-15 times.

f)Test the cleaning efficiency

Model pollution (sebum/makeup - for example, lipstick or mascara) is applied to a specific location on the forearm/person. Plot wash product. For washing RUB soap on the skin for 1 minute, rinse for 30 seconds (for example, at a temperature of 35°C) and dried with a light Pat on the Number of remote dirt/makeup is estimated from the difference in the readings of the device for measuring the intensity of the color, using, for example, Minolta Chromameter®, model CM 2002, taken before and after washing. Alternatively, collect digital images with high magnification and analyzed using the software Optimas® to determine the amount of dirt/makeup removed when washing.

Applying cosmetics

Cosmetics applied to the marked section 3.5 2.5 cm on the inner side of the forearm manner consistent with its normal use. Cosmetic products should be applied in a standardized way to ensure that the loss is approximately equal to the weight of the cosmetics and the floor of the test section is homogeneous. Standards for the application of cosmetics are as follows:

1) liquid cosmetics - up to 20 ml is applied with a pipette to the site and evenly distribute the index finger in a glove;

2) lipstick - three overlapping vigorous smear;

3) pigment eye pencil - three overlapping vigorous smear;

4) mascara - to spread uniformly using a spatula for each coating layer.

Application of pollution

Pollution is put on the marked areas of size 3.5 x 2.5 cm on the inner side of the forearm in the manner described below, which are specific to each individual research if the use of pollution. Application technique pollution tacos is:

1) fat - causing 0.25 g 1.5 g;

2) food - put 0.25 g 1.5 g;

3) protein - causing 0.25 g 1.5 g;

Product testing

A baseline measurement is done using a device for measuring the color intensity of Minoltra Chromameter CM-2002. Then apply makeup or contamination on the identified test sites, as described above.

Measurement using the device are removed again after the cosmetics will dry out for 10 minutes, then makeup/dirt is removed. The standard washing procedure used to remove makeup/dirt, is a 30-second wash with 0.5 ml of liquid product with a 15-second rinsing under running water at a suitable constant temperature (for example, 35°C). When the product is used in the form of impregnated wipes, cloth rubbed in a circular motion for 15 seconds. The last measurement device is removed after makeup/dirt will be removed. This procedure can be carried out twice a day for up to three days. In studies with repeated application, conduct a visual assessment of dryness and redness using standard visual measurement scale, as described above.

g)The smoothness of the skin

The smoothness of the skin is evaluated (clinically) by means of the device Primes® (in vivo optical device that measures the topography of the skin supplied GFM Esstezhnik GmbH, Berlin, Germany is). Measured base roughness (leg/hands - initial dryness degree approximately 1-2). For washing RUB soap on the skin for 30 seconds and the foam leave for 90 seconds, rinse for 30 seconds at 35°C. Again measure the roughness after 30 minutes after the procedure, wash. This procedure can be carried out twice a day up to 5 days.

Smoothness is defined as the average decrease in roughness at the end of the study period. Alternative smoothness of the skin can also be evaluated in the test for the consumers as follows:

The test Protocol for the consumers consists of:

1) selection of approximately 10-20 women in the age group 25-65 from those who use the means to care for a person in the form of soap;

2) the application under test and the comparative products in the course of a week each; half of the participants should apply to first test the product, and the other half must first apply comparative product;

3) at the end of the test, the participants give their preferences (on a scale from 0 to 5 points) on the property, the Skin feels smoother".

Smoothness is defined as consumers ' rating on a scale from 0 to 5 points.

h) Magosti skin

The softness of the skin can be estimated using linear rheometer for skin (Goodyear Scientific Instruments, UK). Exfoliated skin contains less dry scales, therefore, it is softer/less is hard. The test includes basic readings rheometer for skin (foot/hand) to measure the dynamic stiffness constants of the springs (mg/mm) for skin that is associated with the hardness/softness of the skin. For washing RUB soap on the skin for 30 seconds, then lather leave on for 90 seconds, rinse 30 seconds (at a suitable temperature, for example, 35°C) and the skin dry with a light Pat. Following the measurement of the hardness/softness of the skin and hold for 30 minutes after washing. This procedure can be carried out twice a day for up to 5 days. Softness is defined as the average decrease in dynamic stiffness constants of the springs over the study period observed during the study.

Alternative softness of the skin can also be evaluated in the test for the consumers as follows.

The test Protocol consists of:

1) selection of approximately 10-20 women in the age group 25-65 from those who use the means to care for a person in the form of soap;

2) the application under test and the comparative products in the course of a week each; half of the participants should apply to first test the product, and the other half must first apply comparative product;

3) at the end of the test, the participants give their preferences (on a scale from 0 to 5 points) on the property Leather is more delicate.

Softness is determined by assessing consumers HQ the Les from 0 to 5 points

i)Test method pH

To form an aqueous suspension by mixing 10 grams of the formula soap with 90 g of water for the formation of a 10 %suspension. Then measured the pH of the suspension at 25°C.

j)Test method for Zein

Cleansing base toilet soap according to the invention has a solubility of Zein below about 50, 40, 30, and most preferably up to about 25, according to the method of determining the solubility of Zein set forth below. The lower the level of Zein, the product is considered to be softer. This method enables measurement of the solubility of Zein (corn protein grains) in solutions cleansing bases, as follows.

0.3 g of cleansing basics and 29.7 g of water are thoroughly mixed. To this add 1.5 g of Zein and stirred for 1 hour. The mixture is then centrifuged for 30 minutes at a speed of 3000 rpm After centrifugation the pellet is extracted, washed with water and dried in a vacuum oven for 24 hours until almost all the water evaporate. Measure the weight of the dried granules and calculate the percentage solubilizing Zein by the following equation:

% solubilizing Zein = 100 (1-weight of dried granules/1,5).

In addition, % Zein described in the following reference: E. Gotte, "Skin compatibility of tensides measured by their capacity for dissolving zein protein", Proc. IV International Congress of Surface Active Substances, Brussels, 1964, pp 83-90.

k)Organoleptic index exfoliate soap

The body is elepticheskih index exfoliate soap is determined by the following procedure. The consumer takes the soap in one hand and rotates it under running water at 35°C. records the number of rotations required to otshelushivaet to be perceived (i.e. tactile sensations) to the consumer. Index exfoliate soap is defined as the average number of spins required to feel the exfoliating particles in the soap.

1)General Protocol tests on consumers

The test report consists of:

1) selection of approximately 10-20 women in the age group of 25-65 years who are consumers of care products for the face in the form of soap;

2) application of the test and comparative products, each in a week; half of the participants should apply to first test the product, and the other half must first apply comparative product;

3) at the end of the test, the participants give their preferences on a scale from 0 to 5 points according to the following parameters:

exfoliates;

provides gentle exfoliation;

moisturizes and exfoliates;

leather is more delicate;

skin feels smoother;

good for dry skin.

Although this invention has been described in relation to private variants of its implementation, there is no doubt that numerous other forms and modifications of the invention will be obvious to experts in this field. Applied the formula and the invention in General, the om should be interpreted as covering all such obvious forms and modifications which correspond to the true nature and scope of the present invention.

1. Toilet soap containing

a) cleansing base, comprising 20-60 wt.% one or more synthetic detergents surface-active substances;

(b) 10-50 wt.% the humidifier; and

c) exfoliating particles, and at least 25 wt.% particles have an average size, measured along the major axis of the particle, from 100 to 600 microns.

2. Soap according to claim 1, in which the cleaning phase has zeinabou number less than 50.

3. Soap according to claim 1 or 2, in which at least 50% exfoliating particles have an average size, measured along the major axis of the particle, from 100 to 300 microns.

4. Soap according to claim 1, in which the exfoliating particles have a hardness of less than 4 units Mohs, preferably less than 3 units Mohs.

5. Soap according to claim 1, in which the organoleptic index exfoliate soap is less than or equal to 10.

6. Soap according to claim 1, in which the exfoliating particles differ in color from cleansing base.

7. Soap according to claim 1, in which the exfoliating particles are present in the soap at a concentration of less than 1 wt.%.

8. Soap according to claim 1, in which the exfoliating particles larger than 400 μm, preferably more than 300 μm, are at concentrations less than 0.25 wt.%.

9. Soap according to claim 1, in which the exfoliating particles are selected from polyethylene, microcrystalline wax, complex ether is Koby, amorphous silicon dioxide, talc, tricalciumphosphate or mixtures thereof.

10. The soap of claim 1, wherein the humectant is selected from fatty acids, triglycerides, mineral oil, petrolatum, glycerin, polyethylene glycol or mixtures thereof.

11. Soap according to claim 1, in which the ratio of the humidifier to otshelushivaet is in the range from 20:1 to 500:1.

12. Soap according to claim 1, where the soap makes water suspension with a pH of 4 to 8.

13. Soap according to claim 1, additionally containing less than 10 wt.% soluble soap.

14. Soap according to claim 1, obtained by a process comprising a stage

a) preparing at least one synthetic surfactant, at least one humectant, and at least one otshelushivatsya;

b) mixing stage (a) for product education pre-mixture at a temperature sufficient to maintain pre-mixture flowing, or at a higher temperature until the pre-mixture becomes almost uniform, and otslushival and a significant part of the at least one humidifier is not part of the pre-mixture;

c) cooling the resulting product is pre-mixture;

d) optional grinding or refining of chilled product pre-mixture to obtain granules;

e) mixing from the of elusively with a substantial part of one or more humectants, not added to the product of the pre-mixture formed in stage (b) or (C)to obtain exfoliating pre-mixture;

f) mixing exfoliating pre-mixture with the cooled product pre-mixture in the mixing of solids;

g) refining of the product of stage (f)at least once; and

(h) extruding and stamping product in the form of soap.

15. Soap on 14, further comprising a stage of mixing perfumes or simultaneously with otshelushivaet and moisturizer, or as a separate stage to obtain exfoliating pre-mixture.

16. The method of simultaneous exfoliation and hydration of the skin, which includes stages:

a) preparation of soap containing

i) purifying the base, comprising 20-60 wt.% one or more synthetic detergents surface-active substances;

ii) 10-50 wt.% the humidifier;

iii) exfoliating particles, of which at least 25 wt.% have an average size, measured along the major axis of the particle, from 100 to 600 microns;

b) adding sufficient water to wet the soap and skin;

c) applying soap on the skin; and

(d) rubbing soap skin for a time sufficient to remove dead skin cells and covering the lower layer is in the skin at least one humidifier.

17. The method of providing different levels of exfoliation and hydration on different parts of the body of the consumer, which includes stages

a) preparation of soap, and soap includes

i) purifying the basis of containing 20-60 wt.% one or more synthetic detergents surface-active substances;

ii) 10-50 wt.% the humidifier; and

iii) exfoliating particles, of which at least 25 wt.% have an average size, measured along the major axis of the particle, from 100 to 600 microns.

b) hydrating soap, body or both;

c) rubbing the soap user selected area of the skin for a time sufficient to remove dead skin cells, where it is desirable essential exfoliation;

d) adding a sufficient amount of water in the soap to obtain a foam;

e) rubbing foam in user selected skin areas where it is desirable moisture without substantial exfoliation, over time, sufficient to cover the lower layers of the skin at least one humectant, and stage (C) to (e) can be carried out by the user in any order.