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Physical or chemical processes or apparatus in general (B01)

B
Performing operations; transporting
(52506)
B01
Physical or chemical processes or apparatus in general
(8339)

B01B - Boiling; boiling apparatus
(4)
B01D - Separation (separating solids from solids by wet methods b03b, b03d, by pneumatic jigs or tables b03b, by other dry methods b07; magnetic or electrostatic separation of solid materials from solid materials or fluids, separation by high-voltage electric fields b03c; centrifuges b04b; presses per se for squeezing-out liquid from liquid-containing material b30b0009020000)
(4106)
B01F - ixing, e.g. dissolving, emulsifying, dispersing (mixing paints b44d0003060000)
(910)
B01J - Chemical or physical processes, e.g. catalysis, colloid chemistry; their relevant apparatus (processes or apparatus for specific applications, see the relevant places for these processes or apparatus, e.g. f26b0003080000)
(3702)
B01L - Chemical or physical laboratory apparatus for general use (apparatus for medical or pharmaceutical purposes a61; apparatus for industrial purposes or laboratory apparatus whose construction and performance are comparable to that of similar industrial apparatus, see the relevant classes for industrial apparatus, particularly subclasses of b01 and c12; separating or distilling apparatus b01d; mixing or stirring devices b01f; atomisers b05b; sieves b07b; corks, bungs b65d; handling liquids in general b67; vacuum pumps f04; siphons f04f0010000000; taps, stop-cocks f16k; tubes, tube joints f16l; apparatus specially adapted for investigating or analysing materials g01, particularly g01n; electrical or optical apparatus, see the relevant classes in sections g and h);
(88)

Gas-free chamber for fluid media

Invention relates to a device with a chamber for fluid media that may be used in the field of molecular diagnostics, in particular, for polymerase reaction implementation. The chamber for fluid media communicates with the first channel (designed so that to enable implementation of the function of fluid media admission into the chamber for fluid media) and the second channel (designed so that to enable implementation of the function of fluid media release from the chamber for fluid media). The first and the second channels are positioned close to each other with the projection positioned between the first and the second channels projecting into the chamber for fluid media.

Method of removing tritiated water vapour from gases

Method of removing tritiated water vapour from gases includes feeding a gas stream from below a countercurrent phase isotropic exchange column filled with a spirally prismatic filling of stainless steel, and a stream of natural water is fed from the top of the column, wherein the process is carried out at room temperature, and the height of the column is selected based on the required degree of detritisation of the gas.

Method of homogenisation of heat distribution, as well as reduction of amount of nitrogen oxides (nox)

Invention relates to a method of homogenisation of heat distribution, as well as reduction of the amount of nitrogen oxides (NOx) in the combustion products when operating an industrial furnace. The method of homogenisation of heat distribution as well as reduction of the amount of nitrogen oxides (NOx) in the combustion products when operating an industrial furnace with one burner using air as an oxidant. Through the tuyere into the furnace the oxidant is supplied, comprising 50% oxygen gas. The total amount of oxygen supplied is consistent with the amount of fuel supplied through the air burner, at that 40% of the supplied oxygen is injected through the additional oxidant, the tuyere is placed at a distance of 0.3 meters from the air burner, the additional oxidant flow to the furnace is provided through the tuyere with a velocity of sound, the additional oxidant is supplied only when the air burner is operated with a certain minimal or higher power.

Filtration device for treatment of water and other fluids

Proposed device comprises two ceramic filtration membranes and their holders. Said ceramic filtration membranes are shaped to plates, each comprising active filtration outer side and one inner filtered water discharge channel. The holder comprises receiving chamber to discharge water fed from discharge channels and receiving devices for tight securing of ceramic filtration membranes thereat so that inner discharge channels are communicated with said receiving chamber. Part of holder comprising receiving devices for ceramic filtration membranes is composed by one-piece formed part.

Uzm-35 zeolite composition, method of production and methods of use

Invention relates zeolite synthesis. A new family of crystalline aluminosilicate zeolite compositions is synthesised. The UZM-35 composition has a three-dimensional skeleton and contains MFI, ERI and MSE zeolites. The UZM-35 zeolite composition has the empirical formula: M m n + R r + A l ( 1 − x ) E x S i y O z , where M is a combination of ion-exchange potassium and sodium cations, R is a single-charge organoammonium cation, such as a dimethyldipropylammonium cation, and E is a skeleton element such as gallium. The obtained composition is similar to MCM-68 but is distinguished by a specific X-ray diffraction pattern.

Method of producing sorbent for extracting mercury compounds from aqueous solutions

Invention relates to production of sorbents for extracting mercury compounds from aqueous solutions Disclosed is a method of producing a sulphur-containing sorbent which includes polycondensation of sodium polysulphide with an organochlorine compound on the surface of petroleum coke particles. The organochlorine compound used is 1,4-dichlorobutyne-2.

Method of obtaining secondary amides by carbonylation of respective tertiary amines

Invention relates to method of obtaining secondary amides. Method is realised by carbonylation of respective tertiary amines by means of carbon monoxide in presence of catalyst, containing less than 750 parts per million (ppm) of palladium, and halogen-containing promoter.

Composition of charge for high-porosity ceramic material with latticed-cellular structure

Composition of a charge for high-porosity ceramic material with latticed-cellular structure for catalyst carriers comprises an inert filler - electrically molten corundum and disperse phase with a strengthening additive. At the same time to increase material strength, they use a high-aluminous porcelain mass as a disperse phase, and the strengthening additive is a composition MgO+SiC, providing for formation of the phase of eutectic composition in the system MgO-SiO2 when baked in the temperature range of 1250-1300°C with the following ratio of components: electrically molten corundum - 5-20 wt %, high-aluminous porcelain mass - 76.5-90 wt %, strengthening additive MgO+SiC - 3.5-5 wt %.

Gas purification system

Gas purification system comprises a housing, filters, a metal box, a ventilator, the metal box having an inlet opening and tapering in the lower part, a metal gauze placed over the inlet opening and the tapering, a metal mesh filter in form of mesh wire systems placed in the box, having a positive and a negative potential, and two pull in electromagnetic relays are placed at the corners of the box, a membrane filter is placed over the metal mesh filter before the inlet of the ventilator. Furthermore, a control panel has indicators for on/off switching, filling of the metal box, filter cleaning and the end of filter cleaning, as well as a switch.

Device and method for continuous skimming separation of mix containing one or several alkanolamines

Invention is designed for continuous distillation separation of the mix containing one or several alkanolamines. This application describes devices and methods of continuous distillation separation of the mix containing one or several alkanolamines. Separation is performed in one or several columns with web while alkanolamines are extracted as side running.

Device for gas-fluid extraction and method of gas-fluid extraction

Invention relates to fluid treatment. Proposed device comprises phase components feed and discharge means and tubular flow extraction chamber with fluid and carrier gas feed and discharge pipes. Extraction chamber is placed vertically in thermostat. It features hydrophilic inner surface and taper at top end aligned with capillary pipe so that a round slot is formed, or with funnel furnished with hollow cone secured so that a circular slot is formed between funnel surface and cone surface. Gas unions are arranged at acute angle to chamber axis while relative to chamber surface they are fitted tangentially. Method of extraction comprises feed of components into extraction chamber in countercurrent and discharge of carrier gas therefrom enriched in volatile components. Note here that tubular extraction chamber temperature is stabilised. Fluid flow forced into said chamber is converted into coaxial flow flowing over its concave surface in thin film while carrier gas flow is swirled in upward spiral. Mass exchange is executed at countercurrent of phase components or at stationary has phase.

Gas-fluid extraction process and coaxial mass exchanger to this end

Invention is intended for gas-fluid extraction. Proposed method comprises management of fluid and carrier gas flows, formation of phase interphase and mass exchange with subsequent separation of extracted fluid and carrier gas enriched in volatile components. Fluid axial flow incoming to the chamber is transformed into two coaxial flows separated by carrier gas. Extraction in analytical systems is carried in one step whereat fluid and gas phases migrate or in two steps. First, sample is forced via chamber at stationary gas phase normal or decreased pressure. Then, at concentration phase equilibrium, formed cloud saturated with volatile components of carrier gas vapour-gas mix is pushed from said chamber into analyser gas cell whereat carrier gas pressure equals barometric pressure. Device comprises flow-through tubular mass exchange chamber arranged vertically and having coaxial cavity with hydrophilic surface connected at top end with diverging coaxial slit.

Method for optimisation of functioning of device for hydrocarbon synthesis from synthesis-gas by control of partial co pressure

Invention relates to field of synthesis of hydrocarbons from synthesis-gas mixture. Invention deals with method for optimisation of functioning of zone of hydrocarbon synthesis from raw material, which contains synthesis-gas, in which catalyst, containing cobalt, is present, with claimed method including the following stages: a) determination of theoretic value of partial pressure of carbon monoxide in reaction zone, b) regulation of partial CO pressure, determined at stage a), to value, higher or equal 4 bars, c) determination of new value of theoretic value of partial CO pressure CO in reaction zone.

Method of sewage purification from suspended substances and petroleum products

Invention can be applied for purification of surface sewages and oil-polluted industrial discharges. To realise method purified water is preliminarily processed with flocculant with hydrophorbising properties. Then water successively passes stages of sedimentation of sand and large particles, fine mechanic purification from suspended substances, sorption of free and emulsified oil products, additional sorption of soluble oil products on sorbent with fixed microflora. Preliminary introduction of flocculant with hydrophorbising properties reduces load on sorbent, which makes it possible to reduce its volume. Stage of fine mechanic purification is carried out in layer of charge, which consists by 25-35% of the total charge height, made from cylindrical rings with diameter 10-40 mm with ratio of length to diameter (1-2):1, filled in bulk. Additional sorption of soluble oil products is carried out on sorbent with fixed microflora with supply of air oxygen. Dose of flocclulant with hydrophobilising properties constitutes 0.5-2.5 mg per 1 l of processed sewages. Supply of air oxygen is realised with consumption of 1-5 volumes of air per 1 volume of sorbent. Supply of air contributes to more effective regeneration of sorbent with fixed microflora, which makes it possible to prolong term of its service.

Method of producing catalyst for polymerisation of lactones or polycondensation of alpha-oxyacids

Disclosed is a method of producing a catalyst by reacting tin metal with oxyacids, wherein catalyst synthesis is carried out in a melt or solution of oxyacids in the presence of oxidising agents at temperature of 20-240°C while stirring constantly. The oxidising agents used are air or molecular oxygen or hydrogen peroxide or organic hydroperoxides. The α-oxyacids used are compounds with ratio of hydroxyl to carboxyl groups in the range of 1(3):3(1). Condensation of oxyacids with removal of the released water can be carried out concurrently or consecutively with catalyst synthesis.

Adsorbent for drying gases

Adsorbent for drying gases has a porous matrix and, in the pores of the matrix, an active water-absorbing substance from a group of sodium or potassium hydrophosphates or dihydrophosphates with particle size of 1-10 nm in amount of 40-100 wt % with respect to the dry substance of the matrix. The porous matrix used is mesoporous silicates from the group of silicate MCM-41, aluminosilicate, zirconosilicate or titanosilicate with mesopore size of 2-50 nm and overall mesopore volume of not less than 1-2 cm3/g, obtained via sol-gel synthesis or template synthesis. The sodium or potassium hydrophosphates of dihydrophosphates are added by impregnation from a 1 M aqueous solution, followed by drying the adsorbent on air at 100°C for 2 hours. After saturation with water, the adsorbent retains the texture of dry granular material.

Method of obtaining microcapsules of medications of cephalosporin group in konjac gum in toluene

Invention relates to pharmaceutical industry, in particular to method of obtaining microcapsules of medications of cephalosporin group. Method of obtaining microcapsules of medications of cephalosporin group consists in the following: surface-active substance is added to konjac solution in toluene, after that, powder of preparation of cephalosporin group is dissolved in dimethylformamide and transferred into solution of konjac in toluene, after formation by antibiotic of its own solid phase carbinol and distilled water are added in drops, obtained suspension of microcapsules is filtered, washed with acetone and dried, with process of obtaining microcapsules being carried out under specified conditions.

Method for sorption extraction of molybdenum

Invention relates to selective extraction of heavy metal ions, particularly molybdenum (VI) ions, from solutions. Extraction is carried out using a sorbent in form of powdered aluminium oxide by providing contact of the sorbent with a solution at pH 1-7. The sorbent used is then recovered via contact thereof with aqueous potassium sulphate solution at pH 4-6. After recovery, the sorbent separated from the phosphate solution is washed and dried. The recovered sorbent is ready for reuse.

Method of natural gas cleaning and recovery of one or more adsorbers

Method relates to natural gas cleaning by adsorbers and to recovery of the latter. Proposed method comprises forcing the stock containing natural gas through first adsorber to get the product including cleaned natural gas, recovery of second adsorber at heating stage and recovery of second adsorber at cooling stage. Heating stage comprises separation of a portion of stock contained in regeneration gas, feed of the latter into dehumidifier to remove water. Then, performed are regeneration gas heating and regeneration gas feed into second adsorber for its recovery. Cooling stage comprises, at the start of cooling stage, feed of at least a portion of fluid located in second adsorber to dehumidifier for water desorption from dehumidifier molecular sieve and, then, cooling of second adsorber.

Catalyst for producing synthetic base oil and method for preparation thereof

Invention relates to a catalyst for producing synthetic base oil from oligomerisation of hexane-1, having a catalytically active component in form of chromium which is deposited on a support, wherein the support used is silica gel with particle size of 2.2-4.0 mm, pore size of not less than 100 and specific surface area of not less than 300 m2/g, wherein the content of chromium is in the range of 1-3 wt %. The invention also relates to a method of preparing the catalyst, which comprises depositing chromium on silica gel by impregnation with an organic solution of a chromium salt, drying the catalyst at room temperature for 2-3 hours, activating with air at temperature of 500-600°C for 3-5 hours and reducing the catalyst at temperature of 300-350°C in a carbon monoxide current for not less than 2 hours.

Catalyst system for trimerisation of ethylene to alpha-olefins

Catalyst system includes a complex of chromium with a diphosphine ligand of general formula [(Ph2PXPPh2)Cr(THF)Cl3] or [(Ph2P(1,2-C6H4)PPh(1,2-C6H4)CH2OC2H5)]CrCl3, where X is selected from: a hydrocarbon biradical or a substituted hydrocarbon biradical, and also includes methylaluminoxane (activator) and trimethylaluminium (coactivator). Components of the system are in the following molar ratio: chromium complex:activator:coactivator = 0.12-0.13% : 24.97-42.22% : 57.66-74.91%.

Method of activating methane aromatisation molybdenum-zeolite catalyst

At the first step, the catalyst is heated in a hydrogen stream to temperature of 675…725°C and held at said temperature for 1…4 hours; at the second step, the catalyst is cooled to temperature not higher than 50°C and held at said temperature in a medium of an inert gas for 0.5…3 hours; at the third step, the catalyst is reheated in a hydrogen stream to temperature of the first step and held at said temperature for 0.5…2 hours.

Vibration mixer

Vibration mixer comprises a mixing chamber, a rotor with blades, a vibrator rigidly fixed in the centre of the mixing chamber. The vibrator's casing is made as a metal shell being a corrugated thin-walled body of rotation which in the vertical plane section provides for a complex truncated geometric figure by corrugation peaks points, the figure is formed by mean intersection of four circles with the centres being the vertices of a square and with the radiuses being equal to the diagonal of the said square. A disk is rigidly fixed inside the shell in the centre in the horizontal plane, it is fitted with a cylindrical protrusion able of being inserted and fastened along the inner diameter of a spring installed so that it can be freely compressed and released in a cup. A connecting rod driven by the upper crank mechanism is rigidly attached to the centre of the cup's upper inner part, and a pusher is attached to the centre of the cup's upper outer part, the pusher is rigidly coupled by the other end with the inner upper part of the metal corrugated shell. The disk provides for the possibility of generating vibrations from the central part of the vibrator casing with the help of four pushers which by their upper part are symmetrically attached to the lower part of the disk and by the lower part are coupled in a movable pivot unit of the connecting rod of the lower crank mechanism.

Vibration mixer

Vibration mixer comprises a mixing chamber, a rotor with blades. In the top and bottom parts of the chamber, two vibrators are set in the centre and rigidly fixed: the lower and upper vibrators are made in casings and generate vibrations by lower and upper crank mechanisms respectively. The vibrators' casings are made as identical metal shells being corrugated thin-walled bodies of rotation which in the vertical plane section provide for complex truncated geometric figures by corrugation peaks points, the figures are formed by mean intersection of four circles with the centres being the vertices of a square and with the radiuses being equal to the diagonal of the said square. Disks with guide posts are rigidly fixed inside each shell and are set in the centre in the horizontal plane. The disks of the lower and upper vibrators are provided with cylindrical protrusions able of being inserted and fastened along the inner diameter of the springs installed so that they can be freely compressed and released in cups, connecting rods are rigidly attached to the centres of the cups' inner parts, and pushers are attached to the centre of the cups' outer parts, the pushers are rigidly coupled by the other end with the inner parts forming the smallest corrugations out of the metal corrugated shells' corrugations. Four protrusions are symmetrically set on the outer cylindrical parts of the cups. A spring vibration generator made as a spring set is installed in the centre between the casings of the lower and the upper vibrators, the spring set consists of at least two springs of different diameter which are fixed along the diameters of recesses formed on the outer surface of the metal corrugated shells by the set of the smallest corrugations out of the corrugations of the lower and upper vibrators.

Vibration mixer

Vibration mixer comprises a mixing chamber, a rotor with blades. In the top and bottom parts of the mixing chamber, two vibrators are set in the centre and rigidly fixed: the lower and upper vibrators are made in casings and generate vibrations by lower, central and upper crank mechanisms. The vibrators' casings are made as metal shells being corrugated thin-walled bodies of rotation which in the vertical plane section provide for complex truncated geometric figures by corrugation peaks points, the figures are formed by mean intersection of four circles with the centres being the vertices of a square and with the radiuses being equal to the diagonal of the said square. Inside the lower vibrator shell a disk is set in the centre in the horizontal plane and is rigidly fixed, the disk is fitted by a cylindrical protrusion able of being inserted and fastened along the inner diameter of a spring installed so that it can be freely compressed and released in a cup, a connecting rod driven by the central crank mechanism is rigidly attached to the centre of the cup's upper inner part, and a pusher is attached to the centre of the cup's upper outer part, the pusher is rigidly coupled by its other end with the inner upper part of the lower vibrator casing shell. The lower vibrator disk provides for the possibility of generating vibrations of the central part of the lower vibrator casing with the help of four pushers which by their upper part are symmetrically attached to the lower part of the disk and by the lower part are coupled in a movable pivot unit of the connecting rod of the lower crank mechanism. Inside the upper vibrator shell a disk with a guide post is set in the centre in the horizontal plane and is rigidly fixed, the disk is fitted by a cylindrical protrusion able of being inserted and fastened along the inner diameter of a spring installed so that it can be freely compressed and released in a cup, a connecting rod is rigidly attached to the centre of the cup's inner part, and a pusher is attached to the centre of the cup's outer part, the pusher is rigidly coupled by its other end with the inner upper part of the upper vibrator shell forming the smallest corrugation. Four protrusions are symmetrically set on the outer cylindrical part of the cup.

Rotor-type hydraulic hammer

Proposed hammer comprises casing (1) with inlet and outlet pipes (2) and (3), working chamber (15), inner rotor (4) with rotary pump blades (5) and cylindrical ring (6). Slotted diffusers (8) are arranged over the edges of cylindrical ring (6). Outer rotor (10) of countercurrent rotation concentrically covers the inner rotor (4). Outer rotor (10) is equipped with confusers (13) arranged over edges of its cylindrical ring (11). Said hammer is equipped with extra cylindrical rings (7, 12) on inner and outer rotors with diffusers (9) and confusers (14) arranged over their edges. Cylindrical confusers on outer rotor feature smaller diameter compared with cylindrical ring diffusers on inner ring. Extra effects of hydraulic shock on ground material in one pass and series of resonance loads in compression-rarefaction cause fast destruction of grinding material particles.

Adsorption method by kochetov

Adsorption method implies that a gas flow for cleaning is supplied to the lower part of an apparatus through a distribution grid, then it is passed through the external and internal perforated cylinders between which adsorbent is placed, the cleaned gas flow is withdrawn from the adsorber via a connecting pipe, and the waste adsorbent is removed via a discharge gate, the desorption is carried out by supplying the water vapour to a bubbler via the connecting pipe, the bubbler is fitted by perforated toroidal surface for smoother desorption process along the whole height of the perforated cylinders, the adsorbent is made as a cylindrical ring with two hemispherical surfaces being attached to its side surface opposite to each other so that diametral planes of the hemispheres coincide with the upper and lower bases of the cylindrical ring respectively, and the apices of the hemispherical surfaces are set on the ring axis and are turned to each other, and perforation is provided on the side surface and on the hemispherical surfaces.

Scrubber packed bed by kochetov

Packed bed for a scrubber comprising a casing with branch pipes for dust-laden and purified gas, a nozzle spraying device, packing supports with a packed bed in between, and a sludge removing device; the packed bed is made as cylindrical rings and a packed bed element is made as a cylindrical ring with two hemispherical surfaces being attached to its side surface opposite to each other so that diametral planes of the hemispheres coincide with the upper and lower bases of the cylindrical ring respectively, and the apices of the hemispherical surfaces are set on the ring axis and are turned to each other, and perforated surface of nth order, for example, spherical, elliptic, hyperbolic one, is located between the apices of the hemispherical surfaces of the packed bed element.

Hydraulic ash catcher - heat recovery unit

Hydraulic ash catcher - heat recovery unit comprises an inlet pipe branch, a casing, an outlet pipe branch, a settling chamber being filled with water up to the level of a partition wall immersed in the chamber, the lower part of the partition wall is fitted by longitudinal grooves with permanent pitch, an inlet gas duct is equipped by a water sprinkler made as a manifold with nozzles, a pipeline, a screw pump, a tank to collect water, an overflow opening with regulated gate valve, a discharge pipe branch, a tubular coil, each of the nozzles comprises a case fixed on the manifold and a throttle opening with a chamber, and the case is made from two parts coaxial to each other: the base and the cover which are rigidly attached to each other by means of four latches, and an inlet pipe branch creating vortex head pressure in the nozzle case is tangentially attached to the base. The cover plate is volume-type as to evolvent profile with a central conical hole, with a cone apex angle equal to 130°, and the base is shaped, and has a central fairing of vortex flow, which is formed by the conical surface transforming into a sphere at the apex directed towards the central conical hole in the cover, and the base of the conical surface is smoothly adjacent to the toroidal surface of the base.

Apparatus for treating water via crystallisation method

Apparatus has a housing (5), inside of which there is a sealed variable-volume vessel (10), in the top part of which there is a filter (4) for separating heavy water crystals, above which there is an opening (3) for outlet of light water. The filter (4) is attached to the housing (5). Between the filter (4) and the bottom of the vessel (19), having a hose for inlet of water (14) to be treated, there are hollow rings (18), inside of which there are heat exchangers (12), having the shape of Archimedes' spirals connected by flexible hoses in series, and the rings themselves are connected to each other by flexible sleeves (11). The cavity of the lower heat exchanger (12) is linked by a flexible hose (14), which passes through the wall of the housing, with the inlet cavity for the heat carrier (16), having a temperature control device (15) and connected to the volume (17) of the housing (5). The cavity of the top heat exchanger (12) is connected through a valve (6) to the cavity of the outlet pipe for the heat carrier (8), having a temperature control device (7) and linked through a valve (9) to the cavity (17) of the housing (5).

System with centrifugal separator and method of control in such system

Set of inventions relates to system comprising sealed centrifugal separator and to method and control in said system. Proposed system controls characteristics of separated heavy component in sealed separator and includes said separator. Note that separator comprises rotor with separation chamber, inlet channel for components to be separated, first and second channels for discharge of one heavy component and one light component. Note here that system comprises extra means to circulate a portion of separated heavy component from second discharge channel to separation channel. First means to monitoring density, flow rate of combination of said parameters of heavy component in second discharge channel. First control means adjusts circulation flow rate in response to control signal from said first monitoring means. In compliance with this method, control over characteristics of separated heavy components in said system first, mix of components is fed from inlet channel to separation chamber. Thereafter mix of components is separated in separation chamber to light and heavy components. Then, at least one light component is fed to first discharge channel and at least one heavy channel is fed to second discharge channel. Thereafter, portion of separated heavy component is returned from second discharge channel into inlet channel. First means monitoring density, flow rate of combination of said parameters of heavy component in second discharge channel to generate control signal in response to said parameters for control purposes.

Method of oil fractionation

Proposed method comprises heating of oil by vapours of hydrocarbon vapours, heating it in the furnace, stripping of the wide fraction of hydrocarbons with production of fractionation residue and processing of said fraction. Oil is pre-divided into two parts, one being heated by vapours of vacuum gas oil and another one being heated by vapours of said fraction. Both parts are mixed, at least one part of said mix is heated by vapours of the first stage of fractionation while fractionation is performed in three steps. At first step, oil is stripped by gaseous products of vacuum gas oil and vacuum residue processing to get vapours and residue. At second step, vapours of the first fractionation step are subjected to partial condensation by oil cooling for production of heavy gas oil fraction and vapours to be condensed by oil cooling for production of second fractionation stage and wide fraction of hydrocarbons. At third step, residue of the first fractionation stage is mixed with liquid product of vacuum gas oil processing and subjected to vacuum separation to get vacuum residue. The latter are withdrawn from the plant for further processing to get gaseous products and residue as well as vacuum gas oil vapours to be condensed by cooling for production of vacuum gas oil and uncondensed gases to be extracted with the help of evacuation device. Vacuum gas oil is heated by its vapours, mixed with heavy gas oil fraction and derived from the plant to get gaseous and liquid products.

Method of producing phenylethynyl derivatives of aromatic compounds

Method includes heating a mixture of components - 0.01 mol phenylacetylene, 0.01 mol iodobenzene (aryl iodide), 0.0006 g copper nanopowder and 0.002 g CuI at temperature of 110-120°C for 3 hours; after cooling, the reaction mass is poured into 100 ml cold water while stirring, followed by extraction with ethyl acetate, purification on a column with silica gel, elution with a solvent mixture with ratio of ethyl acetate to hexane of 1:6 and then distilling off the solvent to obtain pure products.

Silicon-humus soil ameliorant

Invention relates to environmental conservation technologies, cutting-edge agricultural technologies and chemistry of organosilicon compounds and can be used to restore the structure of disturbed soils by stabilising water-stable aggregate. In particular, the present invention employs water-soluble humic silanol derivatives that are modified in a special way to endow them with the capacity to be irreversibly sorbed on surfaces of mineral particles and other hydroxyl-containing carriers. Humic derivatives are added to the degraded soil in form of aqueous solutions.

Method of producing granular filter charge for process filters for treating water from open water supply sources

Method of producing filter charge for process filters for treating water includes crushing sedimentary rock and firing in high-speed conditions. The sedimentary rock used is limestone which contains calcium carbonate, magnesium carbonate, organic impurities, clay inclusions and quartz.

Method of conversion of carbon oxides

Invention relates to catalyst, suitable to application in reactions of conversion of carbon oxides, in form of granules, formed by pressing reduced and passivated catalyst powder, and claimed powder contains copper in the interval 10-80 wt %, zinc oxide in the interval 20-90 wt %, aluminium oxide in the interval 5-60 wt % and, optionally, one or several oxide promoter compounds, selected from compounds of Mg, Cr, Mn, V, Ti, Zr, Ta, Mo, W, Si and rare-earth elements, in quantity in the interval 0.01-10 wt %. Said granules have average crush strength in horizontal direction after production ≥6.5 kg, ratio of values of average crush strength in horizontal direction after reduction and after production ≥0.5:1 and area of copper surface over 60 m2/g Cu. Invention also relates to method of claimed catalyst production and to method of conversion of carbon oxides in presence of claimed catalyst.

Vibration mixer

Vibration mixer comprises a mixing chamber with the ports for loading and unloading of materials respectively, a rotor with blades and rotary drive. In the top and bottom parts of the mixing chamber, lower and upper vibrators made in casings are set in the centre and rigidly fixed. The vibrators' casings are made as metal corrugated shells being corrugated thin-walled bodies of rotation which in the vertical plane section provide for complex truncated geometric figures by corrugation peaks points, the figures are formed by mean intersection of four circles with the centres being the vertices of a square and with the radiuses being equal to the diagonal of the said square, the shells are able of generating three vibration fields identical in amplitude and different in frequency, two of the fields in the aggregate and one field separately correspond by shape to the corrugated contour of the said bodies of rotation, with differently directed oscillations. Inside the metal corrugated shell of the lower vibrator a disk is set in the centre in the horizontal plane and is rigidly fixed, the disk is fitted by a cylindrical protrusion able of being inserted and fastened along the inner diameter of a spring installed so that it can be freely compressed and released in a cup, a connecting rod driven by the central crank mechanism is rigidly attached to the centre of the cup's upper inner part, and a pusher is attached to the centre of the cup's upper outer part, the pusher is rigidly coupled by its other end with the inner upper part of the metal corrugated shell of the lower vibrator casing and is provided with the possibility of generating vibrations from the upper part of the lower vibrator casing via the connecting rod by the central crank mechanism. The lower vibrator disk provides for the possibility of generating vibrations of the central part of the lower vibrator casing with the help of four pushers which by their upper part are symmetrically attached to the lower part of the disk and by the lower part are coupled in a movable pivot unit of the connecting rod of the lower crank mechanism. A disk with a guide post is rigidly fixed inside the metal corrugated shell in the centre in the horizontal plane. Four protrusions are symmetrically set on the outer cylindrical part of the cup. A spring vibration generator made as a spring set is installed in the centre between the casings of the lower and the upper vibrators, the spring set consists of at least two springs of different diameter which are fixed along the diameters of recesses formed on the outer surface of the metal corrugated shells by the set of the smallest corrugations out of the corrugations of the lower and upper vibrators. It is provided for the generation of three vibration fields with different frequencies in the whole volume of the mixer's mixing chamber for concrete mix components being mixed, along with the simultaneous possibility of providing for the effect of the said vibration fields' overlapping in the centre of the mixing chamber, simultaneous generation of differently directed oscillations in the three-frequency range which prevent the formation of dead zones in the mixing chamber completely, provision of additional vibration action on the mixed components, homogeneous amplitude distribution of each vibration field in the mixing chamber and qualitative intensification of mixing process for these components on the whole.

Heat-resistant nanofibre filter material and method for production thereof

Heat-resistant nanofibre filter material has an internal working layer and two external protective layers placed on both sides of the working layer. The working layer is made by electrical forming from polydiphenylene phthalide fibre with diameter of 200-400 nm and has mass per unit area of 0.5-3.5 g/m2. Protective layers with mass per unit area of 6-8 g/m2 are made from nonwoven quartz material with fibre diameter of 1-7 mcm. Electrical forming of nanofibres of the working layer is carried out in an electric field with strength of 2-6 kV/cm from polydiphenylene phthalide in cyclohexanone, which contains an additive selected from tetraethylammonium and tetrabutylammonium halides. The nanofibres formed are deposited on a substrate made of protective nonwoven quartz material, after which a second protective layer of the same nonwoven material is deposited on the working layer. The disclosed method can be carried out using devices for electrocapillary techniques of electrical forming or devices for electrical forming techniques with a free surface Nanospider™.

Method of organic waste gasification and device for its realisation

Invention relates to wastes processing and gasification of organic material. Device includes gasification chamber with regulated input of technological air and output of raw synthesis-gas, combustion chamber, which provides technological heat in said primary gasification chamber, which contains primary burner, supply of raw synthesis-gas and regulated input of combustion air for burning said raw synthesis-gas, and scrubber for purification of cooled waste gas from said combustion chamber, temperature sensor for measuring temperature of said waste gas before cooling, and regulator for bringing into action said primary burner, when temperature of said waste gas is indicator of temperature of higher risk of dioxin formation.

Vibration mixer

Vibration mixer comprises a mixing chamber, a rotor with blades. In the top and bottom parts of the mixing chamber, two vibrators are set in the centre and rigidly fixed: the lower and upper vibrators are made in casings and generate vibrations by lower and upper crank mechanisms respectively. The vibrators' casings are made as identical metal shells being corrugated thin-walled bodies of rotation which in the vertical plane section provide for complex truncated geometric figures by corrugation peaks points, the figures are formed by mean intersection of four circles with the centres being the vertices of a square and with the radiuses being equal to the diagonal of the said square. Disks with guide posts are rigidly fixed inside each shell and are set in the centre in the horizontal plane. The disks of the lower and upper vibrators are provided with cylindrical protrusions able of being inserted and fixed along the inner diameter of the springs installed in cups, connecting rods are rigidly attached to the centres of the cups' inner parts, and pushers are attached to the centre of the cups' outer parts, the pushers are rigidly coupled by the other end with the inner parts of the metal corrugated shells forming the smallest corrugations. Four protrusions are symmetrically set on the outer cylindrical parts of the cups.

Rotary extractor

Invention can be used in radiochemical production for cleaning and separation of radioactive fluids, and in chemical, metallurgical and pharmaceutical industries. Rotary extractor comprises housing with mixing chamber, light phase discharge chamber and heavy phase discharge chamber with partition, rotor with separation chamber and conveying device, hydraulic lock and light phase discharge pipes and drive mounted at housing cover. Top part of heavy phase discharge chamber is equipped with the pocket secured to housing inner wall. Aforesaid partition arranged concentrically in gap between said pocket and drive is connected with housing cover. Partition bottom edge is located under pocket top edge while said cover is a turning design.

Sublimation apparatus for fine purification of substances

Sublimation apparatus for fine purification of substances has a heat-insulated heated cover, a heated housing, a sublimation chamber, a desublimation chamber divided into cells by parallel partition walls, arranged with spacing relative to the cover, a heat carrier chamber, a raw material inlet pipe, a process gas outlet pipe, heat carrier inlet and outlet pipes. The housing heater is made of self-contained blocks lying in each cell of the housing. The heat carrier chamber is made of sections, each lying in a cell. The heat carrier inlet pipes have a check valve. A self-contained block is a high-frequency generator.

Vibration mixer

Vibration mixer comprises a mixing chamber, a rotor with blades, a vibrator rigidly fixed in the centre of the mixing chamber, with the drive for vibration generation from a crank mechanism. The vibrator's casing is made as a metal corrugated shell being a corrugated thin-walled body of rotation which in the vertical plane section provides for a complex truncated geometric figure by corrugation peaks points, the figure is formed by mean intersection of four circles with the centres being the vertices of a square and with the radiuses being equal to the diagonal of the said square. Inside the shell a disk with a guide post is set in the centre in the horizontal plane and is rigidly fixed, the disk is fitted by a cylindrical protrusion able of being inserted and fastened along the inner diameter of a spring installed so that it can be freely compressed and released in a cup, a connecting rod is rigidly attached to the centre of the cup's upper inner part, and a pusher is attached to the centre of the cup's upper outer part, the pusher is rigidly coupled by its other end with the inner upper part of the metal corrugated shell. Four protrusions are symmetrically set on the outer cylindrical part of the cup.

Vibration mixer

Vibration mixer comprises a mixing chamber, a rotor with blades. In the top and bottom parts of the mixing chamber, two vibrators are set in the centre and rigidly fixed: the lower and upper vibrators are made in casings and generate vibrations by lower and upper crank mechanisms respectively. The vibrators' casings are made as identical metal shells being corrugated thin-walled bodies of rotation which in the vertical plane section provide for complex truncated geometric figures by corrugation peaks points, the figures are formed by mean intersection of four circles with the centres being the vertices of a square and with the radiuses being equal to the diagonal of the said square. Disks with guide posts are rigidly fixed inside each shell and are set in the centre in the horizontal plane. The disks of the lower and upper vibrators are provided with cylindrical protrusions able of being inserted and fixed along the inner diameter of the springs installed so that they can be freely compressed and released in cups, connecting rods are rigidly attached to the centres of the cups' inner parts, and pushers are attached to the centre of the cups' outer parts, the pushers are rigidly coupled by the other end with the inner parts forming the smallest corrugations out of the metal corrugated shells' corrugations. Four protrusions are symmetrically set on the outer cylindrical parts of the cups. A spring is installed between the casings of the lower and upper vibrators along the diameters of recesses formed by the smallest corrugations out of the corrugations of the metal corrugated shells at the lower and upper vibrator casings.

Method of cleaning of gases and sulphur-bearing gas extraction

Invention relates to removal of sulphur-bearing gases from unrefined gases. Note here that removed sulphur-bearing gases are processed gases at high regeneration pressure. This allows the feed of sulphur-bearing gases into storage with lower costs for compression. Unrefined gas is fed to absorption tower to it to be cleaned of sour gas components with the help of physical absorbent. Absorbent saturated with sulphur-bearing gases and those suitable for use is, then, fed in high-pressure stripping tower for evaporation of the portion of absorbent and production of extraction steam. Extraction steam is used for separation of co-absorbed gases suitable for use. The latter are output from high-pressure stripping tower top end. Absorbent contained in vapours of stripping tower top end is liquefied and derived back into high-pressure stripping tower. Absorbent flow from bottom end of said tower is fed to high-pressure regeneration tower for separation of sulphur-bearing gases and derivation at high pressure in regeneration tower top end. Regenerated absorbent is derived from said bottom end into absorption tower.

Magnetically controlled sorbent agent for bilirubin elimination from biological fluids

Invention refers to medicine and is applicable for treating endogenous intoxication caused by high plasma bilirubin concentrations accompanying various pathologies. Substance of a method: a surface of a magnetically controlled sorbent agent is coated with hydrophobic ligands either in the form of 3-mercaptopropionic acid methyl ester, or in the form of polymeric octadecylhydrosilicic acid, or in the form of polymeric hydrosilicic acid, containing covalently attached octadecyl ligands. Magnetite micro- and nanoparticles are presented by Fe3O4. The total bilirubin recovery rate in the sorbent agent is determined by a lyophilised bovine serum dry powder. The bilirubin content is determined by formula: AB(%)=100-(A460 nm test/A460 nm reference)×100, wherein AB(%) is a percentage of the absorbed bilirubin; A460 nm test is an optical density of the solution contacted the sorbent agent; A460 nm reference is an optical density of the solution before contact with the sorbent agent; 460 nm is a wave length whereat bilirubin has the maximum optical absorption.

Method of producing adsorption element

Invention relates to methods of producing an adsorption element. The method includes preparing a starting composition of a crystalline adsorbent selected from zeolite, silica gel or a combination thereof, mixing with a polymer binder in form of polymers of fluorinated derivatives of ethylene. A rheological additive is added to the obtained mixture. The suspension of adsorbent powder and the polymer binder in the rheological additive is moulded into a raw article of given shape. The raw moulded article is either subjected to heat treatment in a vacuum or is exposed to a microwave field until the rheological additive is removed. The end surfaces of the adsorption element are then coated with the suspension of the adsorbent and the polymer binder in the rheological additive or the rheological additive and the adsorption elements are exposed under normal conditions in an air atmosphere. The end surfaces of at least two adsorption elements are brought into contact and the point of contact is either subjected to heat treatment or is exposed to a microwave field.

Method of producing recoverable carbon dioxide absorber

Invention relates to a method of producing a recoverable carbon dioxide absorber. The method includes reacting basic zirconium carbonate and zinc oxide. The basic zirconium carbonate is fed for reaction with moisture content of 20-24 mol/kg. Granules are formed using acrylic lacquer as a binding agent in amount of 3-7% with respect to dry substances.

Electrochemical water pump

Proposed pump comprises solid-polymer electrolysis cells and fuel cells hydraulically communicated via water collection tank. The latter has water inlet union, oxygen and hydrogen gas separators hydraulically communicated with appropriate cavities of electrolysis cells and, pneumatically, with appropriate cavities of fuel elements. Note here that oxygen gas separator is hydraulically communicated with water collection tank. Hydrogen gas separator is equipped with water discharge union. Note also that electrolysis cells and fuel cells are connected by power electric circuit.

Device for compacting, mixing and graining of bulk materials

Device for compacting, mixing and graining of bulk materials comprises a feeder, a receiving hopper, a horizontal endless conveyor belt, support rollers disposed under its upper branch, an inclined endless perforated tape mounted over the horizontal endless conveying belt, both belts are stretched on drums connected to drives of rotational motion, the support rollers of the horizontal endless conveyor belt are made in the form of a roller track disposed under its entire upper branch, transverse blades with a height of 10…40 mm and a step of 100…200 mm are mounted on the inclined endless perforated tape, in the area of its contact to the horizontal endless conveyor tape there is a horizontal area with a length of 0.2…0.3 of its width and a curved reflector with fluid injectors is installed over its upper branch along the entire tape width, and fixed enclosing walls are attached from the outer lateral sides of both tapes.

Another patent 2513823.

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